BSB
BOD
DBO
BOD BOD measurements according to DIN Measurement BOD measurement according to EN 1899-1 and EN 1899-2 and for self-checks
Biological Oxygen Demand The Biological Oxygen Demand is an important parameter in water resource management. It is a quantity used for the quality of water and the purification power of biological wastewater treatment stages. In addition it is essential in the planning and dimensioning of sewage treatment plants. In routine use BOD determination is used to check the wastewater in the inflow and discharge of sewage treatment plants. Depending on the measurement site and type of wastewater the BOD value can lie between a few mg/l and several thousand mg/l. Several methods are available for carrying out the measurement. WTW offers various measuring systems for these methods. In “dilution BOD” the oxygen content of a sample is measured with an oxygen sensor before and after an incubation period of 5 days. The difference between the measurements is the BOD5 value; this method is officially recognized. In “BOD self-checks” with the respirometer the reduction in oxygen causes a definite pressure difference which can be measured by a pressure sensor. This method is very easy to carry out and is a practical method. As these two methods are basically very different they only correlate for a few samples which, however, have a practical relevance such as in the discharge channels of municipal sewage treatment plants. In both cases the samples must be kept at 20 °C for 5 days. WTW offers a wide range of suitable thermostatted equipment.
Seminars WTW offers seminars in which the subject of BOD measurement is treated in detail. On request WTW will be pleased to send you further details about these seminars.
Literature Further information on this subject can be requested from WTW:
BOD primer (CD-ROM) Application reports Offprints
108 Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
Laboratory & Field General Features
BOD Measurement
pH
“Dilution BOD”
ORP
according to EN 1899-1 (previously DIN 38 409 P51) and EN 1899-2 from page
inoLab® BSB/BOD Level 3 Versatile, accurate, with evaluation program 110 acc. to EN 1899-1, EN 1899-2 and ISO 5815-1989 Comfortable, robust, accurate
113
OxiTop® IS 12
OxiTop®
Simple handling, 5-day memory, mercury-free pressure measurement
114
OxiTop® Control
Comfortable, large memory, infrared data transmission, graphics display
118
Extension sets and Accessories
❍ OxiTop® measuring heads + SETs ❍ OxiTop® control system
123 123
(measuring heads, controller...) 124 125 125
❍ Thermostat boxes ❍ Thermostat cabinets
126 127
Photometry
Thermostats
❍ Stirrer platforms ❍ Storage racks, marking rings ❍ General accessories
Applications from page
For documentation
For applications for soil analysis, biodegradability and others please refer to the Oxygen consumption rate section
130
Software, printers and accessories
180
Customer Service
OxiTop® Control
BOD
from page
Turbidity
Model
Respiration Sample Preparation
practical method according to the self-check regulations (previously DIN 38 409 P51)
Colony Counter
“BOD self-check measurement”
MultiParameter
Conductivity
Oxygen (D.O.)
ProfiLine Oxi 197, ProfiLine Oxi 197-S
Software, Printers
inoLab® BSB/BOD Level 3
ISE
with instrument
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
109
BSB
BOD
DBO
EN 1899-1/ 1899-2
“Dilution BOD”
according to EN 1899-1 (previously DIN 38 409 P51) and EN 1899-2
BOD5 measurements can be carried out with all WTW laboratory oxygen meters. The instruments as the complete range of accessories are described in the “oxygen meters” section.
With inoLab® BSB/BOD Level 3 flexible and powerful inoLab® BSB/BOD Level 3 with terminal, self-stirring StirrOx® G oxygen sensor and bar-code reader
NEW
110
IP 43
3 Year Warranty
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
StirrOx® G
Laboratory & Field ORP ISE BOD
MultiParameter
Self-stirring oxygen sensor – simultaneous stirring and measurement
Colony Counter
Optionally a PC keyboard or bar-code reader can be connected for sample identification
• For a detailed description of further oxygen meters in the inoLab® family • Complete range of accessories
see page 66 ff. see page 70 ff.
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
Customer Service
Software, Printers
Turbidity
Photometry
● Single-handed operation for rapid series measurements ● Constant approach flow for high reproducibility ● Immediately ready for measuring – no polarization period required ● Extremely low self-consumption of oxygen - only 0.008 µg h-1 (mg/l)-1 ● Zero-current free – no zero point calibration necessary ● With calibration and storage vessel OxiCal®-ST as standard ● Long working life – 6 months with one electrolyte filling ● IMT temperature compensation with 2 built-in temperature sensors ● Membrane leakage monitoring – damaged membranes are indicated
Oxygen (D.O.)
• BOD/depletion • Determination of the biochemical oxygen demand according to DIN EN 1899-1 • Determination of oxygen depletion according to DIN 38 414 P6 • Up to 5 samples for dilution water • Up to 30 measuring samples • Up to 18 dilutions per measuring sample • Up to 7 routines can be stored • Adjustable incubation time, 5 ... 30 days
Conductivity
This laboratory oxygen meter has been specially developed for BODn measurements. A special program allows BODn determination according to EN 1899-1. You can store up to 7 of your own routines for frequently occurring dilution ratios. A maximum of 30 measuring samples each with 18 dilutions allow the management of up to 540 diluted samples. The inoLab® BSB/BOD Level 3 can also be used as a conventional high-end oxygen meter.
Special functions
Respiration Sample Preparation
Versatile – precise – with BODn evaluation program
pH
General Features
“Dilution BOD” according to EN 1899-1 (previously DIN 38 409 P51) and EN 1899-2
111
BSB
BOD
DBO
Technical Data inoLab® BSB/BOD Level 3 Measuring range/ Resolution
O2 conc.
Temperature
0.00 ... 19.99 mg/l 0.0 ... 90.0 mg/l* 0.0 ... 199.9% 0 ... 600%* 0.0 ... 199.9 mbar 0 ... 1250 mbar -5.0 ... +50.0 °C
Accuracy (±1 digit)
O2 conc. O2 saturation Temperature
±0.5% of value ±0.5% of value ±0.1 K
Temp. compensation
0 ... +50 °C automatic via IMT compensation
Salinity correction
Automatic from 0.0 ... 70.0, adjustable via display
O2 saturation O2 part. press.
* depends on oxygen sensor and medium
AutoRead
For reproducibility better than 0.05 mg/l or better than 1 mbar pO2
Real-time clock
Not affected by power cuts
KCalibration
OxiCal® rapid calibration in OxiCal®-SL
Data memory
2000 Data sets (measurement, temperature, time/date, ident no.); time-controlled storage at intervals from 1 s ... 60 days, data storage period unlimited BSB/BOD: max. 540 diluted samples and multiple dilution water
Data output
Via display or interface
Interface
Self-configuring as analog output 0-2 V or bidirectional RS 232
Other connections
For StirrOx® G with automatic AutoRead start and stop via key on StirrOx® G
Operating time
Continuous from mains supply
Protection type
IEC 529 / IP 43
Dimensions (B x D x H in mm)
300 x 250 x 70
Weight
Approx. 1.5 kg
Certified to
CE, TÜV/GS, UL, CUL
Warranty
3 years on the instrument
Ordering Information BOD measurement with inoLab® BSB/BOD Level 3
Order No.
inoLab® BSB/BOD Level 3 Flexible and powerful – the intelligent BOD measuring place consisting of multifunction box and universal terminal, with PC software/connection cable
1H30-010
inoLab® BSB/BOD Level 3 Intelligent BOD measuring place with additional built-in printer
1H31-010
inoLab® BSB/BOD Level 3 The integrated BOD measuring place, with PC software/connection cable, without printer/terminal
1H32-000
KF 12
Karlsruhe bottle including 60 mm ground stopper, suitable for BOD5 determination, minimum order 10 bottles
205 700
Ordering Information SETs inoLab® BSB SETs
Order No.
inoLab® BSB/BOD Level 3 Including terminal, oxygen sensor and accessories
1H30-011
inoLab® BSB/BOD Level 3 With built-in printer, including terminal, oxygen sensor and accessories
1H31-011
inoLab® BSB/BOD Level 3 Without printer/terminal, with PC software/connection cable, sensor and accessories
1H32-001
Accessories CellOx® 325-3 StirrOx G
Galvanic oxygen sensor, 3 m cable Self-stirring oxygen sensor
2 4
Bar-code reader SET ordering example
2
inoLab® BSB/BOD Level 3 + CellOx® 325-3
1H30-011
2
Note: other sensors in SET and instruments versions for 120 VAC/60 Hzs are available on request
112
Please refer to page 70 for oxygen sensors and page 74 for further accessories. Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
Laboratory & Field General Features
“Dilution BOD” according to EN 1899-1 (previously DIN 38 409 P51) and EN 1899-2
pH
With ProfiLine Oxi 197, Oxi 197-S
ORP
comfortable · robust · accurate
Ordering Information BOD measurement with ProfiLine Oxi 197 and Oxi 197-S
Order No.
ProfiLine Oxi 197
ProfiLine oxygen meter, extremely robust, hose-water proof (IP 66), RS 232 digital output, operation from mains supply or rechargeable batteries, with plug-in power supply with connection for self-stirring oxygen sensor StirrOx® G and CellOx® 325
200 350
ProfiLine Oxi 197-S
As ProfiLine Oxi 197, but additionally with 2 analog recorder outputs corresponding to the display of oxygen and temperature
200 313
StirrOx® G
Self-stirring oxygen sensor for oxygen determination in Karlsruhe bottles, with OxiCal®-ST calibration and storage vessel and accessory case with spare parts and maintenance supplies
201 425
KF 12
Karlsruhe bottle including 60 mm ground stopper, suitable for BOD5 determination, minimum order 10 bottles
205 700
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
Colony Counter Turbidity
Photometry
see page 64 ff. see page 70 ff.
Software, Printers
• Detailed description of the ProfiLine Oxi 197 and Oxi 197-S laboratory oxygen meters • Complete range of accessories
3 Year Warranty
Customer Service
IP 66 IP 67
Respiration Sample Preparation
BOD
MultiParameter
Conductivity
Oxygen (D.O.)
ISE
Laboratory oxygen meters ProfiLine Oxi 197 and ProfiLine Oxi 197-S with self-stirring oxygen sensor StirrOx® G
113
BSB
BOD
DBO
BOD “BOD Self-Check Measurement Measurements” Practical method according to the self-check regulations Proposal for a German standard method – DEV 46th installment 2000 – H55 OxiTop® IS 6, OxiTop® IS 12
U.S. patent granted (US 5,770,153)
1 Year Warranty Mercury-free BOD measurement
Features Simple handling Mercury-free measurement 5-day memory Push-button measurements possible Extendable Mobile Precise
Despite all discussions about quicker alternative methods, the determination of the biological oxygen demand BOD has not become any less important. On the contrary, it is still one of the most important measurements for the management of water resources and allows statements to be made about the loading of waters and wastewater with biodegradable substances. The importance of the respirometric BOD measurement is also shown by the inclusion of the “Determination of the biochemical oxygen demand after n-days (BODn) in a respirometer – extension of the method according to DIN EN 1899-2 (H55)” as a proposal for a German standard method in the 46th installment 2000 of the DEV.
Criticisms of the conventional manometric measuring systems have mainly concerned the use of mercury for measuring the pressure. Mercury is toxic and if not handled properly it produces vapors which are injurious to health. With the development of the OxiTop® systems, WTW has fulfilled a worldwide customer wish – mercury-free BOD determinations. With OxiTop® WTW now offers a unique and modular mercury-free BOD instrument system which has been developed for daily practical use. OxiTop® alters the previous handling process in a revolutionary manner.
114 Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
General Features
OxiTop® IS 6, IS 12
Laboratory & Field
“BOD self-check measurements”
pH
Complete package for 6 or 12 measuring places
ORP
The OxiTop® IS 6, IS 12-6 and IS 12 complete packages have been assembled so that they contain everything necessary to carry out the measurements.
ISE
OxiTop® IS 6
Oxygen (D.O.)
Ready for use with 6 measuring places
OxiTop® IS 12-6
Conductivity
Ready for use with 6 measuring places, extendable to 12 places
MultiParameter
OxiTop® IS 12 Ready for use with 12 measuring places
Conversion to OxiTop® Any conventional manometric BOD measuring instrument (no matter whether from WTW or anybody else) can be converted to the OxiTop® system. Various conversion sets are available. (see page 123)
Customer Service
Test agents see page 125
Respiration Sample Preparation
... or conversion
Colony Counter
1 Stirrer platform IS 6/IS 12 with plug-in mains power supply (see page 124) 1 REF 600 Stirrer bar remover 1 NHP 600 NaOH pellets 1 NTH 600 Nitrification inhibitor 1 MK 164/600 Overflow flask 164 ml 1 MK 432/600 Overflow flask 432 ml 1 Dia/600 Chart paper block
Photometry
Each package contains:
1 Year Warranty
Turbidity
OxiTop® (green or yellow) PF 600 Amber sample bottle GK 600L Rubber sleeve RST 600 Stirrer bar
Software, Printers
1 1 1 1
BOD
Each measuring place contains the following items:
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
115
BSB
BOD
DBO
¡ OxiTop® closely observed BOD measurement with “brains” US patent granted (US 5,770,153) Registered industrial property rights: • Protected design patent • Utility model patent
The patented measuring head contains the following items: ● 1 Piezoelectric pressure sensor ● 2 Operating keys: M for showing the momentary value; S for showing the stored value ● 2-place LED, displaying 00 to 50 “scale divisions”. 1 scale division corresponds to 3.55 hPa. A correct measurement should only show scale divisions up to 40; with larger values the sensible measuring range has already been exceeded so that the display only serves for orientation purposes. ● Data memory for 5 measurements at daily intervals. It is not necessary to read off the measurements every day as they are made automatically. This means that measurements can be carried out over a weekend with unattended operation. The measurement can also be read off after 7 days (BOD7). ● AutoTemp function: delayed start of measurement for samples which are too cold. OxiTop® delays the start until a constant temperature has been achieved; the minimum delay period is 1 hour. ● 2 batteries with a typical working life of 1 year (if properly used for BOD measurements).
Very modern microelectronics Pressure sensor, microcontroller, timer, memory
IP 54
1 Year Warranty
Technical Data OxiTop®-measuring head Measuring principle
Manometric with pressure sensor
Quantity measured
BODn
Measuring range
0 ... 40 digits (display units) equals 0 ... 40 / 80 / 200 / 400 / 800 / 2000 / 4000 mg/L BOD
Display range
0 ... 50 digits
Display accuracy
±1 digit (^ = ±3.55 hPa)
Display
2-character 7-segment LED, 10 mm
Operating range
500 ... 1100 hPa
Memory
For BOD, daily
Power supply
Lithium battery (280 mAh) 2 x CR 2430
Power consumption
Max. 25 mA (during display of measurements)
Safety class
3 to IEC 1010
Protection type
IP 54 to DIN 40 050
EMC
EN 61326 Class B, FCC Class A
Climate class
2, VDI/VDE 3540
Ambient temperature
Storage: -25 ... +65 °C Operation: +5 ... +50 °C
Dimensions
69 x 70 mm (H x dia.)
Test certificates
CE, TÜV/GS, UL, CUL
Warranty
1 year on the instrument
116 Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
Laboratory & Field General Features
“BOD self-check measurements”
pH
Ordering Information Order No.
Complete package, ready for use, for 6 measuring places, with IS 6 Inductive Stirring System, for mains operation 230 V / 50/60 Hz and 6 OxiTop® measuring systems, including 6 sample bottles, 6 rubber sleeves, 6 stirrer bars and other accessories
208 210
OxiTop® IS 12-6
Complete package, ready for use, for 6 measuring places (extendable to 12 measuring places), with IS 12 Inductive Stirring System, for mains operation 230 V / 50/60 Hz and 6 OxiTop® measuring systems, including 6 sample bottles, 6 rubber sleeves, 6 stirrer bars and other accessories
208 212
OxiTop® IS 12
Complete package, ready for use, for 12 measuring places, with IS 12 Inductive Stirring System, for mains operation 230 V / 50/60 Hz and 12 OxiTop® measuring systems, including 12 sample bottles, 12 rubber sleeves, 12 stirrer bars and other accessories
208 211
ORP
OxiTop® IS 6
OxiTop® IS 6
Accessories
from page
OxiTop® IS 6 and OxiTop® IS 12
System extensions Conversions (OxiTop® measuring heads, stirring systems IS 6, IS 12) Storage rack for OxiTop® Marking rings
123 123 125 125
Thermostatic instruments (boxes, cabinets)
126 Customer Service
For system
Software, Printers
Accessories
Turbidity
Photometry
Colony Counter
OxiTop® IS 12
Respiration Sample Preparation
BOD
MultiParameter
Conductivity
Oxygen (D.O.)
Note: versions for 120 VAC / 60 Hz on request
ISE
BOD determination with OxiTop® “mercury-free” measuring system
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
117
BSB
BOD
DBO
BOD “BOD Self-Check Measurement Measurements” Practical method according to the self-check regulations Proposal for a German standard method – DEV 46th installment 2000 – H55 OxiTop® Control 6, OxiTop® Control 12
1 Year Warranty
Features Comfortable handling Mercury-free pressure measurement Large data memory in measuring head Infrared data transmission to controller Automatic sample management Automatic measuring protocol Mobile Precise
118
Comfortable BOD determination with the OxiTop® Control system The OxiTop® Control system is the logical further development of the successful OxiTop® system. • Instead of the display and keys the OxiTop®-C measuring head has an infrared interface with which it communicates with Controller OC 100 or OC 110. • The Controller OC 100/OC 110 can manage up to 100 OxiTop®-C measuring heads.
The measuring head stores 180 to 360 data sets (depending on set running time) which can be called up at any time in the Controller and where they are shown graphically. Call-up is by collect call or selectively by “pointing” to the required measuring head. Each measuring head has its own identification; this means that manual identification is no longer necessary.
• Documentation is carried out via the Achat OC program in combination with a PC (or the TD 100 Thermal printer)
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
General Features
Operation
• Set running time
• Wait until set running time has elapsed • If necessary, monitor sample by calling up the data (can also be carried out through glass or Plexiglas,
• When measurement is finished result can be read off from the Controller display • Documentation of results
Conductivity
OxiTop® Control
ORP
• Data can be called up as often as required during the measurement
ISE
• Incubate sample
so that the sample is not disturbed by opening the door of the thermostat cabinet!)
Oxygen (D.O.)
• Set operating mode either BOD routine for single samples or BOD standard for samples with parallel batches and statistical evaluation
• Prepare sample and start measurement by briefly clicking the measuring head with the Controller
pH
Operation of the system is clear and simple • Select language
Laboratory & Field
“BOD self-check measurements”
Complete package for 6 or 12 measuring places
MultiParameter
The OxiTop® Control 6 and Control 12 complete packages have been assembled so that they contain everything necessary to carry out the measurements.
BOD
OxiTop® Control 6
Respiration Sample Preparation
Ready for use with 6 measuring places
OxiTop® Control 12 Ready for use with 12 measuring places
Each measuring place contains the following items:
Photometry
Colony Counter
OxiTop®-C PF 600 Amber sample bottle GK 600L Rubber sleeve RST 600 Stirrer bar
Software, Printers
1 Controller OC 100 1 Stirrer platform IS 6/IS 12 with plug-in mains power supply (see page 124) 1 REF 600 Stirrer bar remover 1 NHP 600 NaOH-pellets 1 NTH 600 Nitrification inhibitor 1 MK 164/600 Overflow flask 164 ml 1 MK 432/600 Overflow flask 432 ml 1 Dia/600 Chart paper block
Turbidity
Each package contains:
1 Year Warranty
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
Customer Service
1 1 1 1
119
BSB
BOD
DBO
¡ OxiTop®-C closely observed BOD measurement with “infrared brains”
The measuring head with its protected design and utility model patents contains the following items: ● 1 Piezoelectric pressure sensor, pressure range 500 to 1350 hPa ● Infrared interface for data transmission to Controller with pilot lamp ● Data memory for max. 360 data sets. Data is stored automatically at preset time intervals from 0.5 hours to max. 99 days. ● AutoTemp function: delayed start of measurement for samples which are too cold. OxiTop®-C delays the start until a constant temperature has been achieved; the minimum delay period is 1 hour. In the BOD standard operating mode this function can be switched off. ● 2 batteries with a typical working life of 1 year.
1
IP 54
1 Year Warranty
Technical Data OxiTop®-C measuring head Measuring principle
Manometric with pressure sensor
Measurement of
BODn
Pressure range
500 ... 1350 hPa
Accuracy
± 1% of value ± 1 hPa
Resolution
1 hPa (corresponds to 0.7% of BODn measuring range)
Display
LED pilot lamp
Power supply
2 x CR 2430 lithium batteries (280 mAh)
Safety class
3, IEC 1010
Protection type
IP 54 to DIN 40 050
EMC
EN 61326 Class B, FCC Class A
Climate class
2, VDI/VDE 3540
Ambient temperature
Storage: -25 ... +65 °C Operation: +5 ... +50 °C
Dimensions
70 x 70 mm (H x dia.)
Test certificates
CE, TÜV/GS, UL, CUL
Warranty
1 year on the instrument
2
120
1
Short click from controller to measuring head to start the sample
2
Infrared call-up of data at incubator. Data transfer even through closed incubator doors and OxiTop® boxes
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
General Features
¡ OxiTop® Control closely observed
Laboratory & Field
“BOD self-check measurements”
pH
The handy Controller manages the data for up to 100 OxiTop®-C measuring heads.
ISE
OC 110 only:
Conductivity
Oxygen (D.O.)
OC 100/OC 110: 0 ... 40 / 80 / 200 / 400 / 800 / 2000 / 4000 mg/L BOD (corresponds to 0 ... 142 hPa) • measuring range variable with upper limit 400 000 mg/L (in BOD special mode) • 500 ... 1350 hPa (pressure mode)
Data sets per measurement
180 ... 360 (depends on running time)
Measurement period
Adjustable from: 0.5 ... 6 h in 0.5 h steps 6 ... 24 h in 1 h steps 1 .. 99 days in 1 day steps
Display
LCD graphics display 64 x 128 point
Energy supply
3 x 1.5 V alkaline batteries (AA/mignon)
Safety class
3, IEC 1010
Protection type
IP 42 to DIN 40 050
EMC
EN 61326 Class B, FCC Class A
Climate class
2, VDI/VDE 3540
Ambient temperature
Storage: -25 ... +65 °C Operation: +5 ... +40 °C
Dimensions
45 x 100 x 200 mm (H x B x D)
Weight
Approx. 390 g
Test certificates
CE, TÜV/GS, UL, CUL
Warranty
1 year on the instrument
Achat OC PC communication program, TD 100 thermal printer Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
Respiration Sample Preparation
Measuring ranges
Colony Counter
● AutoTest with function monitoring and system messages ● High data security, independent of power supply from batteries
Controller OxiTop® OC 100 + OC 110
Photometry
Confidence in the measurements is guaranteed by:
Technical Data
Turbidity
● Large graphics display ● Operator guidance in - German, English, French, Spanish, Italian (OC 100) - German and English (OC 110) ● Data transmission even through glass doors ● Simple adaptation to specific measuring tasks
Software, Printers
Operating comfort guaranteed by:
BOD
MultiParameter
1 Year Warranty
IP 54
Customer Service
● Identifying the samples with automatic number allocation, i.e. manual marking or labeling the samples is not necessary ● Data call-up function for all samples or selected samples. ● Sample progress display ● Calculation, evaluation and graphical presentation of BOD value ● Protocol of data on batteryoperated TD 100 Printer or with a PC via the Achat OC communication program
ORP
This comprises:
121
BSB
BOD
DBO
Ordering Information BOD determination with Controller OxiTop® OC 100 and OxiTop®-C measuring heads “mercury-free” OxiTop® Control 6
Order No.
Complete package, ready for use, for 6 measuring places, with Controller OC 100 and IS 6 Inductive Stirring System, 208 201 for mains operation 230 V / 50/60 Hz and 6 OxiTop®-C measuring systems, including 6 sample bottles, 6 rubber sleeves, 6 stirrer bars and other accessories
OxiTop® Control 12 Complete package, ready for use, for 12 measuring places, with Controller OC 100 and IS 12 Inductive Stirring System, for mains operation 230 V / 50/60 Hz and 12 OxiTop®-C measuring systems, including 12 sample bottles, 12 rubber sleeves, 12 stirrer bars and other accessories
208 204
Note: versions for 120 VAC / 60 Hz on request
Accessories
Order No.
TD 100
Thermal printer (battery-operated) with IR interface for data transmission from Controllers OxiTop® OC 100 and OC 110 including 1 roll of special paper and 1 set of batteries
208 900
RP 100
1 roll of special paper for TD 100 thermal printer (minimum order 5 rolls)
208 910
Software
(see also page 180)
Order No.
ACHAT OC
PC communication program “ACHAT OC” for Controller OxiTop® OC 100 or OC 110 for further data processing and documentation of measuring data. Software requirements: Windows 3.1 or higher, update possibilities on request. Required accessory: interface cable AK 540/B
208 990
AK 540/B
Interface cable for connecting Controller to a PC via the RS 232 interface, including 9/25-pole adapter
902 842
Test agents see page 125
Accessories for system
Accessories
OxiTop® Control 6 System extensions OxiTop®-C IS 6, IS 12 and Storage rack for OxiTop® OxiTop® Control 12 Thermostatic instruments (boxes, cabinets)
from page 123 125 126
122 Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
Laboratory & Field
“BOD self-check measurements”
General Features
BOD System Extensions, Measurement Conversions,
ORP
pH
general accessories
ISE
System extensions and conversions
2 OxiTop® measuring heads (1 yellow, 1 green)
208 814
OxiTop®/GB
1 OxiTop® measuring head (yellow)
208 810
OxiTop®/GN
1 OxiTop® measuring head (green)
208 800
OxiTop® measuring heads in SETs with accessories
Order No.
OxiTop® SET-2
SET for 2 measuring units, complete with 2 OxiTop® measuring heads (1 yellow, 1 green), 2 sample bottles, 2 sleeves, 2 magnetic stirrer bars
208 819
OxiTop® SET-6
SET for 6 measuring units, complete with 6 OxiTop® measuring heads (3 yellow, 3 green), 6 sample bottles, 6 sleeves, 6 magnetic stirrer bars
208 817
OxiTop® SET-10
SET for 10 measuring units, complete with 10 OxiTop® measuring heads (5 yellow, 5 green), 10 sample bottles, 10 sleeves, 10 magnetic stirrer bars
208 818
OxiTop®-C measuring heads and SETs OxiTop®-C IS 6 / IS 12 extension sets for OxiTop® Control With the extension sets OxiTop®-C IS 6 and OxiTop®-C IS 12 the OxiTop® Control instruments can be extended by 6 and 12 measuring units respectively.
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
BOD
208 812
OxiTop®-2
Respiration Sample Preparation
6 OxiTop® measuring heads (3 yellow, 3 green)
Colony Counter
208 813
OxiTop®-6
Photometry
10 OxiTop® measuring heads (5 yellow, 5 green)
Turbidity
Order No.
OxiTop®-10
Software, Printers
OxiTop® measuring heads
Customer Service
Ordering Information OxiTop®-measuring heads and SETs
MultiParameter
Conductivity
The OxiTop® measuring systems can be used to convert all conventional BOD measuring systems in a very simple way.
Oxygen (D.O.)
OxiTop®-measuring heads and SETs
123
BSB
BOD
DBO
Ordering Information OxiTop®-C measuring heads and SETs OxiTop®-C measuring heads
Order No.
OxiTop®-C
1 OxiTop®-C measuring head
208 830
OxiTop®-C 2
2 OxiTop®-C measuring heads
208 823
OxiTop®-C 6
6 OxiTop®-C measuring heads
208 822
OxiTop®-C measuring heads in extension set for OxiTop® Control
Order No.
OxiTop®-C IS 6
Extension set for 6 measuring positions complete with IS 6 inductive stirring system, for mains operation 230 VAC 50/60 Hz, with 6 OxiTop®-C measuring heads and 6 sample bottles, 6 rubber sleeves, 6 magnetic stirrer bars
208 130
OxiTop®-C IS 12
Extension set for 12 measuring positions complete with IS 12 inductive stirring system, for mains operation 230 VAC 50/60 Hz, with 12 OxiTop®-C measuring heads and 12 sample bottles, 12 rubber sleeves, 12 magnetic stirrer bars
208 133
Note: versions for 120 VAC 60 Hz on request
Stirrers for BOD measurement Technical Data IS 6
IS 12
Energy supply
Plug-in mains transformer 230 VAC (+10%...-15%), 50/60 Hz/24 VA optionally for 120 VAC (+10%...-15%), 50/60 Hz/24 VA
No. of stirring positions
6
Stirrer speed
Program-controlled, 180...450 min-1
Safety class
3, IEC 1010
Protection type
IP 30 to DIN 40050
EMV
EN 61326 Class B, FCC Class A
Climate class
2, VDI/VDE 3540
Ambient temperature
Storage: -25 °C...+65 °C Operation: +5 °C...+40 °C
Dimensions (H x B X D)
67 x 265 x 181 mm
67 x 350 x 266 mm
Weight
1.6 kg
3.2 kg
Test certificates
CE, TÜV/GS, UL, CUL
Warranty
1 year on the instrument
12
Stirrers IS 6 and IS 12 have been specially developed for BOD measurement with the OxiTop® system. With the aid of a software-controlled speed alteration system the stirrer always catches the stirrer bar so that it cannot remain stationary nor can it wobble about. The sample is simply placed on a stirrer and the magnetic stirrer bar will start rotating properly in the center without any problems. The speed is selected so that an optimal gas exchange with the sample takes place. The stirrer is maintenance-free and non-wearing as it contains no moving parts.
Ordering Information for stirrers Stirrers
124
Order No.
IS 6
Stirrer for 6 stirrer positions, mains operation 230 VAC, 50/60 Hz
208 140
IS 12
Stirrer for 12 stirrer positions, mains operation 230 VAC, 50/60 Hz
208 141
Note: versions for 120 VAC/50/60 Hz on request Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
Laboratory & Field General Features
Accessories “BOD self-check measurements”
pH
General accessories and spare parts
ORP
Storage racks
ISE
For safe storage of OxiTop® measuring systems and OxiTop®-C measuring heads
Oxygen (D.O.)
Marking rings
209 013
Batt/OxiTop®
Spare batteries (1 set)
209 012
MK 22/600
Overflow measuring flask, contents 22,7 ml
209 030
MK 43/600
Overflow measuring flask, contents 43,5 ml
209 040
MK 97/600
Overflow measuring flask, contents 97,0 ml
209 050
MK 164/600
Overflow measuring flask, contents 164 ml
209 060
MK 250/600
Overflow measuring flask, contents 250 ml
209 070
MK 365/600
Overflow measuring flask, contents 365 ml
209 080
MK 432/600
Overflow measuring flask, contents 432 ml
209 090
PF 600
Sample bottle, amber, minimum order 3 pcs
209 100
GK 600 L
Rubber sleeve, minimum order 3 pcs
209 172
RST 600
Stirrer bars, minimum order 3 pcs
209 120
REF 600
Stirrer bar remover
209 130
NHP 600
Sodium hydroxide pellets, 2 bottles of 50 g
209 140
NTH 600
Nitrification inhibitor
209 331
Dia/600
5 blocks of chart paper
209 020
OxiTop® PM
Test agent for monitoring OxiTop® systems (packing unit for checking 6 measuring systems)
209 333
OxiTop® PT
Test agent for checking under-pressure and leakage for all OxiTop® measuring heads
209 334
Test agents
Mercury disposal HgP 6
Mercury disposal package for 6 measuring positions
209 162
HgP 10
Mercury disposal package for 10 measuring positions
209 163
QBM 600
Mercury binding agent (1 kg)
209 190
PE 600
Rubber ball, fits threads of PF 600 bottle
209 207
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
Respiration Sample Preparation
Set of marking rings (6 pcs) with set of identification shields (1-12) for bottle identification
Colony Counter
209 010
Mark-6
Photometry
Storage rack for 6 OxiTop® measuring systems
Turbidity
Order No.
St-OxiTop®
Software, Printers
General accessories
Customer Service
Ordering Information general accessories
BOD
MultiParameter
Conductivity
For identification of BOD bottles for OxiTop® instruments
125
BSB
BOD
DBO
BOD Thermostats Measurement OxiTop® Box, thermostat cabinets
OxiTop® Box compact – precise
Technical Data OxiTop® Box Energy supply
230 VAC, 50 Hz (+10 ... -15%) optionally 115 VAC 60 Hz (+10 ... -15%)
Power consumption
200 W
Starting current
Max. 5 A (10 A for 115 V, 60 Hz)
Safety class
2, EN 61010
Climate class
2, VDI/VDE 3540
Ambient temperature
Storage: -25 ... +50 °C Operation: +10 ... +32 °C
Temperature control
20 °C ± 1 K
Ventilation
Yes
Additional heating
Yes
Internal sockets
1
CFC-free
Yes
Dimensions
375 x 425 x 600 mm (H x B x D)
Weight
Approx. 30 kg
Test certificate
CE
Warranty
1 year on the instrument
Example of an application: OxiTop® Box with OxiTop® Control 12
Thermostat box with forced air circulation for 20 ± 1 °C OxiTop® Box is a benchtop model with hinged clear-view cover which can accommodate a maximum of either 12 OxiTop® measuring places or 20 Karlsruhe bottles. The chamber is equipped with a connection for an IS 6 or IS 12 stirrer. A special compartment is provided for thermostatting 6 methylene blue samples. The box is made of non-corrosive materials and the compressor is CFC-free. A cross-flow fan ensures uniform temperature distribution. The box has an automatic defrosting system with condensate evaporation.
Ordering Information BOD thermostat boxes OxiTop® Box
126
BOD OxiTop® Box, thermostat box with temperature-controlled forced ventilation for 230 V 50 Hz mains supply
Order No. 208 432
Note: versions for 115 V / 60 Hz on request Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
General Features
Thermostat Cabinets
Laboratory & Field
Thermostats
Sizes /2 and /4 are available with transparent insulating glass doors. Alternatively all thermostat cabinets can be provided with a variable temperature controller, range +5 ... +40 °C.
Customer Service
As the samples must be additionally stirred the thermostat cabinets are fitted with internal sockets to provide the stirrers with electricity.
Depending on the thermostat cabinet size up to 48 samples can be thermostatted simultaneously.
Photometry
BOD5 values must be determined at a constant temperature of 20 °C. If this requirement cannot be realized at the workplace then a thermostat cabinet in which the samples can be placed for the duration of the test is required.
Turbidity
Thermostat cabinets with fixed and variable temperatures
Software, Printers
1 Year Warranty
Colony Counter
Respiration Sample Preparation
BOD
MultiParameter
Conductivity
Oxygen (D.O.)
ISE
ORP
pH
versatile · powerful · inexpensive
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
127
BSB
BOD
DBO
Technical Data TS 606/2
TS 606-G/2
TS 606/3
TS 606/4
TS 606-G/4
TS 1006
Energy supply
230 V/50 Hz Euro
Power consumption
120 W
130 W
140 W
150 W
170 W
150 W
Gross contents
180 l
180 l
260 l
360 l
360 l
500 l
Weight
37 kg
47 kg
46 kg
62 kg
79 kg
76 kg
Ambient temperature
+10 °C...+32 °C
Temperature control
20 °C ± 1 K
Forced air circulation
Yes
Additional heating
Yes
Internal sockets
4 884 x 602 x 600 734 x 513 x 433
1215 x 602 x 600 1589 x 602 x 600 1589 x 602 x 600 1515 x 755 x 715 1047 x 513 x 433 1418 x 513 x 433 1418 x 513 x 433 1338 x 646 x 516
CFC-free Dimensions (H x B x D in mm)
Yes outside: inside:
850 x 602 x 600 734 x 513 x 433
Certified to
CE, TÜV/GS
Warranty
1 year on the instrument
Note: Versions for 120 VAC 60 Hz on request
Technical Data TS 606/2-Var
TS 606-G/2-Var
TS 606/3-Var
TS 606/4-Var
TS 606-G/4-Var
TS 1006-Var
Energy supply
230 V/50 Hz Euro
Power consumption
140 W
140 W
160 W
170 W
190 W
170 W
Gross contents
180 l
180 l
260 l
360 l
360 l
500 l
Weight
37 kg
47 kg
46 kg
62 kg
79 kg
76 kg
Ambient temperature
+10 °C...+32 °C
Temperature control range
+5 °C..+40 °C ±1 K
Forced air circulation
Yes
Additional heating
Yes
Internal sockets
4
CFC-free Dimensions (H x B x D in mm)
Yes outside: inside:
850 x 602 x 600 734 x 513 x 433
884 x 602 x 600 734 x 513 x 433
Certified to
CE, TÜV/GS
Warranty
1 year on the instrument
1215 x 602 x 600 1589 x 602 x 600 1589 x 602 x 600 1515 x 755 x 715 1047 x 513 x 433 1418 x 513 x 433 1418 x 513 x 433 1338 x 646 x 516
Note: Versions for 120 VAC 60 Hz on request
128 Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
TS 606/2-Var
As TS 606/2 but with digital temperature setting in the range +5 ... +40 °C with digital display of actual value
208 365
TS 606-G/2
As TS 606/2 but with insulated glass front doors
208 253
TS 606-G/2-Var
As TS 606-G/2 but with digital temperature setting in the range +5 ... +40 °C with digital display of actual value
208 366
TS 606/3
Thermostat cabinet for 3 BOD instruments OxiTop® Control 6/12/ OxiTop® IS 6 /IS 12-6 / IS 12 / IS 602
208 362
TS 606/3-Var
As TS 606/3 but with digital temperature setting in the range +5 ... +40 °C with digital display of actual value
208 367
TS 606/4
Thermostat cabinet for 4 BOD instruments OxiTop® Control 6/12/ OxiTop® IS 6 / IS 12-6 / IS 12 / IS 602
208 355
TS 606/4-Var
As TS 606/4 but with digital temperature setting in the range +5 ... +40 °C with digital display of actual value
208 368
TS 606-G/4
As TS 606/4 but with insulated glass front doors
208 356
TS 606-G/4-Var
As TS 606-G/4 but with digital temperature setting in the range +5 ... +40 °C with digital display of actual value
208 369
TS 1006
Thermostat cabinet for 4 BOD instruments OxiTop® Control 6/12/ OxiTop® IS 6 / IS 12-6 / IS 12 / IS 602
208 622
TS 1006-Var
As TS 1006 but with digital temperature setting in the range +5 ... +40 °C with digital display of actual value
208 370
Laboratory & Field Customer Service
Software, Printers
Note: versions for 120 VAC 60 Hz on request
BOD
208 252
Respiration Sample Preparation
Thermostat cabinet for 2 BOD instruments OxiTop® Control 6/12, OxiTop® IS 6 /IS 12-6 / IS 12 / IS 602
Colony Counter
Order No.
TS 606/2
Photometry
BOD thermostat cabinets
Turbidity
Ordering Information BOD thermostat cabinets
MultiParameter
Conductivity
Oxygen (D.O.)
ISE
ORP
pH
General Features
Thermostats
Wissenschaftlich-Technische Werkstätten GmbH & Co. KG · Dr.-Karl-Slevogt-Straße 1 · 82362 Weilheim · Germany · Tel.: +49 (0) 881-1 83-0 · Fax: +49 (0) 881-62 53 9
129