Curriculum Vitae Awards Press Releases List of Publications

Professor, Dr. Vijai K. S. Shukla

Professor, Dr Vijai K. S. Shukla is director of International Food Science Centre A/S, Denmark and has been active in food science research since 1969. He has published numerous papers and has authored several books. His research interests have ranged from physical phenomena to mechanisms of autoxidation, isolation of lipids, spectral phenomena related to lipids, modern analytical methodology, and involvement of essential fatty acids in health and diseases such as Multiple Sclerosis and Batten's Syndrome. http://en.wikipedia.org/wiki/Vijai_Shukla

List of contents Curriculum Vitae .................................................................................................................... 3 Contact information and personal data .............................................................................. 3

Professional appointments ............................................................................................. 3 Expertise ............................................................................................................................. 3 Research interests ................................................................................................................ 4 Specialization ....................................................................................................................... 4 Resolving various scientific problems ................................................................................................... 4

Accomplishments in Industrial Applications ..................................................................... 5 Special features of NUTRIDAN ............................................................................................................. 5

Cosmeceuticals .................................................................................................................... 6 Extraordinary achievements ............................................................................................... 6 Appearances and awards ....................................................................................................................... 6

AOCS activities .................................................................................................................... 6 Associate Editor, JAOCS 1992-; Associate Editor, INFORM 1989-97 ............................................ 6

Other ..................................................................................................................................... 7 World Bank ........................................................................................................................... 8 Malaysian assignment ............................................................................................................................ 8

Media Coverage.................................................................................................................... 8 Newspaper, magazine and television ................................................................................................... 8

Awards .................................................................................................................................... 9 Hindi Rattan Award (2016) ................................................................................................... 9 AOCS’s Fellows Award (2005)............................................................................................. 9 AOCS’s Stephen S. Chang Award (2002) ......................................................................... 10 AOCS’s Herbert J. Dutton Award (1996) ........................................................................... 10 AOCS’s Young Scientist Research Award ....................................................................... 10

Research Accomplishments providing global impact in Lipid Research ................... 10 Nutritional significance of lipids in human health and disease ...................................... 10 Encapsulated oils for corrective nutrition ........................................................................ 10 Chocolates and confectionery .......................................................................................... 10 Designer oils ...................................................................................................................... 11 Collaboration with Institutes and other Professors ......................................................... 11

List of Publications ............................................................................................................. 12 1970 - 1980 .......................................................................................................................... 12 1981 - 1990 .......................................................................................................................... 13 1991 - 2000 .......................................................................................................................... 13 2001 - 2010 .......................................................................................................................... 15 2011 - ................................................................................................................................ 136

2 Presentation of Professor, Dr Vijai K S Shukla

Curriculum Vitae Contact information and personal data Name:

Professor, Dr Vijai K S Shukla

Title: President, International Food Science Centre A/S Date of birth: March 23, 1948, Allahabad, UP India Nationality: Danish E-mail:

[email protected]

Websites:

www.ifsc.dk www.icsc.dk www.nutridan.dk www.hippodan.dk

Telephone: Telefax: Address:

+45 86 22 99 86 +45 86 22 99 96 Sønderskovvej 7 DK-8520 Lystrup Denmark

Professional appointments  

President o 1991 – Present

International Food Science Centre A/S, Denmark International Cosmetic Science Centre, Denmark Research & development Manager o 1979 – 1989 Aarhus Oliefabrik, Denmark

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Research & Development Director o 1990 – 1991 Karlshamn, Sweden

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Adjunct Professor o 2000 – 2008

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Adjunct Professor o 2011 – Present

Adjunct Professor o 2012 – Present

Department of Food Science & Human Nutrition University of Illinois – Urbana Champaign Department of Food Science & Nutrition College of Food, Agricultural & natural Resource Science University of Minnesota, St. Paul, Minneapolis Department of Food Science & Nutrition Institute of Food and Agricultural Sciences University of Florida, Gainesville, Florida

Expertise Food: Food design and innovative products with expertise in Lipid Nutrition, Antioxidants and Actives for better and safer health. Stability: Design stable products and optimization of factories in terms of cost economics for industries such as Chocolate, Frying, Dairy and Nutraceutical industries.

3 Presentation of Professor, Dr Vijai K S Shukla

Cosmeceuticals: Design lipid and active based Cosmeceuticals for the industry and provide extensive knowledge in handling and application of these products in formulations. Antioxidants: Development of exclusive tailor made antioxidants for Food, Cosmeceutical and Pharmaceutical industries. Several of these synergistic mixtures have been developed as processing aid antioxidants and providing preservative properties as well. Internal Stabilisation Technology: Unique technique to make all vegetable oils and fats highly resistant to oxidation and general degradation using the natural antioxidant properties of Rosemary.

Tropical Products / Procurement and research: Expertise in developing unique unconventional exotic raw materials from the jungles of Africa and Asia and introduce these to the modern world. These natural materials are incorporated in several of the product portfolios of the multinational companies. Factory Hygiene and Quality Systems: Provide know how for operating parameters for optimization and improving cost economics globally. Ecology: Involved globally in converting conventional product portfolio to Organic as and where possible.

Research interests Professor, Dr Vijai K S Shukla is author of nearly 100 original scientific publications, 12 invited review papers, 15 book chapters in the areas of biochemistry, human nutrition, cosmeceuticals, nutraceuticals, enzymology, modern analytical techniques for the separation of lipids and proteins. Editor of six books.

Specialization Resolving various scientific problems Professor, Dr Vijai K S Shukla's research interests have ranged from physical phenomena to mechanism of autoxidation, isolation of lipids, spectral phenomena related to lipids, modern analytical methodology and involvement of essential fatty acids in health and diseases such as multiple sclerosis and Batten's syndrome. Professor, Dr Vijai K S Shukla has shown essential fatty acid deficiency in multiple sclerosis and Batten's disease. These were related with glutathione peroxidase activity and antioxidants requirements in these diseases. Professor, Dr Vijai K S Shukla has also analyzed arctic diet in Greenland Eskimos and

4 Presentation of Professor, Dr Vijai K S Shukla

compared with Danes elucidating some of the mechanism of coronary heart diseases in these population groups. In his research work Professor, Dr Vijai K S Shukla employs modern analytical methodology in order to resolve various scientific problems

Accomplishments in Industrial Applications Professor, Dr Vijai K S Shukla has been working in the area of confectionery product development for the three decades. He has a special expertise in cocoa butter, milk fat, cocoa butter equivalents and cocoa butter substitutes based on modern concepts of recipe engineering. Professor, Dr Vijai K S Shukla has always applied scientific principles to upgrade or modify existing production to achieve super quality products. Some of his major achievements are as follows: During 1996 Professor, Dr Vijai K S Shukla has established a brand new refinery in The Netherlands and has successfully demonstrated that total oxidation in bulk oils can be completely arrested and speciality fats delivered to the customers will be of extremely fresh quality. These deliveries were in the scale of 5001000 MT per shipment. A proper research approach clearly shows that it is possible to provide uplift to large scale production through extreme caretaking the help of nitrogen as inert gas and stainless steel in the production system. A number of international press articles presented these developments. For last two decades Professor, Dr Vijai K S Shukla’s research focussed on the quality of encapsulated fish and vegetable oils. He has successfully demonstrated that it is possible to produce ultra refined fish oil with extreme low peroxide value and anisidine value. This oil is already in commercial production. Having produced the above mentioned oils it is of utmost importance to keep these oxidation values extremely low therefore he has designed several natural antioxidant systems for general nutrition as well as cosmetic oils. This natural antioxidant system is 50 to 60 times more powerful than existing available antioxidants. He has recently developed a novel designer oil called Nutridan containing very high amounts of essential polyunsaturated fatty acids. The oils used are of vegetable origin and extracted by physical means and are thus totally solvent free. Nutridan provides not only balanced essential fatty acids, but also a high dosage of natural antioxidants which are extremely beneficial for better health. Special features of NUTRIDAN  Extremely low ratio of omega 6 and omega 3 fatty acid, (typically 0,5 – 0,6)  Helps to lower the ratio of omega 6/omega 3 fatty acids in human nutrition  Contains natural herb extracts, which provide various physiological benefits.  Very high oxidative stability. Nutridan can be used for producing various kinds of table spreads, mayonnaise, salad dressings, baking fats etc. It can also be encapsulated for various pharmaceutical applications. Nutridan is now used successfully in several industries within in baking, frying and cooking as a supplement for correcting omega 6/omega 3 nutrition. Both President Nelson Mandela and President Bill Clinton have used this oil for safer and better health.

5 Presentation of Professor, Dr Vijai K S Shukla

Cosmeceuticals Shukla has been working in the area of application of natural lipids such as exotic butters for cosmetic formulations. He has designed a specific method for internally stabilization of exotic lipids through providing enhanced shelf-life of the final product. He has authored several papers related to these topics. He is now re-dressing cosmetics through the power of naturals.

Extraordinary achievements Appearances and awards Appearance in Who's Who in the World, 12th edition 1995-96. Appearance in 2000 Outstanding Scientists of the World. Appearance in 2000 Outstanding Intellectuals of the 20th Century, appearance in The Barons 500 Leaders for the new Century. The Cambridge Blue Book 2005. American Oil Chemists' Society 1996 prestigious Herbert Dutton Award for pioneering contribution in Lipid research presented in Indianapolis. The title of the award lecture was “Chocolate - The Chemistry of Pleasure”. American Oil Chemists’ Society 2002 prestigious Stephen S. Chang Award presented in Montréal, Canada. The title of the award lecture was ”Chocolate – Friend or Foe?” This award is given to a scientist who has achieved decisive accomplishments in basic research. The knowledge that the person has produced must have been utilized by industries for the improvement or development of food products related to lipids. AOCS Fellow 2005 in recognition of his achievements in science and appreciation for significant service to the AOCS.

AOCS activities Associate Editor, JAOCS 1992-; Associate Editor, INFORM 1989-97 Chairman, "Analysis of Lipids" session, at AOCS Annual Meeting, Hawaii, 1986; Chairman, "General Analytical Topics" session, at AOCS Annual Meeting, New Orleans, 1987; Chairman, "HPLC of Lipids and Proteins", at AOCS Annual Meeting, Phoenix, Arizona, 1988; Chairman, International Short Course on "Application of Pulsed NMR Techniques in Food Analysis", Arizona, 1988; Chairman, "HPLC of Triglycerides and Lipids - A Worldwide Perspective", at AOCS Annual Meeting, Cincinnati, 1989; Chairman, "Analysis - General" session, at AOCS Annual Meeting, Baltimore, 1990; Chairman, International AOCS Short Course entitled "New Horizons in the Analysis of Lipids and Lipoproteins" held in Rebild Bakker, July 1990; Chairman, AOCS Short Course "HPLC of Lipids" held in Chicago, 1991; Chairman, "Speciality Fats" for AOCS Annual Meeting, Chicago, 1991; Chairman, "Antioxidants in the Future" for AOCS Annual Meeting, Toronto, 1992; Chairman, "Newer Developments within the Area of Speciality Fats" for AOCS Annual Meeting, Anaheim, 1993; Chairman Timothy L. Mounts Memorial Symposium in St. Louis, Missouri, 2006. AOCS INFORM advisory board from year 1998-2002. Vice Chairman AOCS Chromatography Committee (1987-91); NMR Committee; Divisionalization Committee; Chairman, HPLC of Triglycerides Ringtest Committee. Chairman NMR Committee (1991-2005). Invited speaker for the World Conference on "Edible Oils and Fats Processing" Maastricht October 1-6, 1989 title "Confectionery Fats". Invited speaker for AOCS Short Course, "Analyses of Fats, Oils and Lipoproteins", Chicago, Nov. 1989 titles "Application of HPLC to Lipid Separation and Analysis: Neutral Lipids", "Application of HPLC to Lipid Separation and Analysis: Lipid Derivatives", Application of NMR Spectrometry: Pulsed NMR". Invited award lecture in INFORM on ”Chocolate – the Chemistry of Pleasure”, February 1997. Invited speaker for symposium on Ten-Year Forecast: ”Trends in Global oilseed Utilization and Processing, Chicago, May 1998. Invited speaker and chairman World Conference and Exhibition on Oilseed Processing and Utilization, Cancun, Mexico, 2000. Presented the lecture ”Confectionery Fats”. Presented following papers during various AOCS meetings; "Recent Applications of the High Performance Liquid Chromatography to Oils and Fats Analysis" at AOCS Annual Meeting, Philadelphia, 1985; "HighSpeed Liquid Chromatography as applied to Oils and Fats Analysis" at AOCS Annual Meeting, Hawaii, 1986; "Studies on the Crystallization Behaviour of the Confectionery Fats by Pulse Nuclear Magnetic Resonance Employing Various Tempering Modes" at AOCS Annual Meeting, New Orleans, 1987; "HPLC of Unconventional Oils" at AOCS Annual Meeting, Phoenix, 1988; "HPLC Determination of Amino Acids in 6 Presentation of Professor, Dr Vijai K S Shukla

Leguminous Proteins", Phoenix, 1988; "Application of High Performance Size Exclusion Chromatography (HPSEC) for the Evaluation of Health Food Oils", Cincinnati, 1989. Presented two papers "TLC of Lipids" and "HPLC (normal phase, reverse phase, detection methodology) at the conference "New Trends in Lipid and Lipoprotein Analysis", La Grande Motte, France, 1993, chaired one session. Chairman General Health & Nutrition at AOCS Annual Meeting, Atlanta, 1994. Chairman General Analytical I&II at AOCS Annual Meeting, St. Antonio, USA, 1995. Chairman General Analytical II at AOCS Annual Meeting, Indianapolis, USA, 1996. Chairman General Analytical II at AOCS Annual Meeting, Seattle, USA, 1997. Chairman General Analytical II at AOCS Annual Meeting, Chicago, USA, 1998. Chairman General Analytical I at AOCS Annual Meeting, Orlando, USA, 1999. Chairman General Analytical II at AOCS Annual Meeting, San Diego, USA, 2000. Chairman General Analytical II at AOCS Annual Meeting, Minneapolis, USA, 2001. Chairman Edward G. Perkins Memorial Symposium: New Horizons in Lipid Production and Processing I &II. Salt Lake City, 2005. Correcting Omega-3/Omega-3 Nutrition through Internal Stabilization Technologies. Salt Lake City 2005. Developed Young Scientist Research Award within AOCS in 2000. This award is sponsored by International Food Science Centre A/S from 2000 till date.

Other Member of Programme Advisory Committee, Palm Oil Research Institute of Malaysia; Member of Pennsylvania Manufacturers' Confectioners' Association; Royal Society of Chemistry; The Chromatography Society, England, Chairman "NMR Group", International Office of Cocoa Chocolate and Confectionery; Executive governing board member, Scandinavian Society for Lipid Research; Nominated to AOCS Governing Board member (1991) a rare honour given to a European; Awarded several scientific honours including AOCS award for outstanding paper presentation; Several president's honour roll; Coorganizer, 15th Scandinavian Symposium on Lipids, June 1989, Rebild Bakker Denmark. Invited lectures at several conferences and meetings in USA, Europe, Japan, India, Malaysia; Editor, 15th Scandinavian Symposium on Lipids. Editor, Applications of pulsed NMR Techniques for Food Analyses; Editor, Antioxidants in Food - Past, Present and Future; Editor, Oils and Fats in the Nineties; Editor, Antioxidants, Free Radicals and Polyunsaturated Fatty Acids in Biology and Medicine; Editor, Modern Developments in Food Lipids. Keynote speaker at Leatherhead Food RA conference on fats in England 1995. Keynote speaker at OTAI's International Seminar in Bombay, India December 1995. Speaker at MOSTA's Short Course 1: CTEU, Pahang, Malaysia April 1996. Chairman Society of Chemical Industry Meeting on Confectionery Fats, London October 1996. Plenary lecture OTAI, Lucknow, India, April 1998. Plenary lecture OTAI National Convention, Calcutta, November 1998. Session Chairman during the 23rd World Congress and Exhibition of the International Society for Fat Research (ISF) in Brighton, England, October 1999. Session Chairman during SCI/Euro Fed Lipid Conference in Cambridge, England, April 2002. Society of Cosmetic Chemists’s (SCC) Meeting in LA, Dinner Hour Speaker, April 2005. SCC Scientific Seminar in LA, October 2006 Keynote speaker at HSCG (Handcrafted Soap & Cosmetic Guild) Annual Conference in Tucson, AZ, USA. Title “Nature´s Gift to Soap & Cosmetics”, May 2014 Editorial Board Member: Lipid Technology, UK and Journal of Food Lipids, USA. Ph.D Examiner of theses from Japan, Germany, Denmark and India.

Professor, Dr Vijai K S Shukla had a detailed technical discussion with His Excellency the President of India Dr A.P.J Abdul Kalam atHis 'Rashtrapathi Bhawan office' on 23rd of June 2006 7 Presentation of Professor, Dr Vijai K S Shukla

World Bank Malaysian assignment Expert assignment on behalf of World Bank within Food Technology Area. Developed strategies for Malaysian Prime Minister’s Vision 2020 programme within Food Science research in Malaysia.

Media Coverage Newspaper, magazine and television Professor, Dr Vijai K S Shukla appears frequently in international newspapers, magazines and recently Times of India sent their senior feature writer to write several articles about his work and Danish Television (DK4) made a programme about his recent research discoveries. European Tribute Professor Fritz Spener, Past-President of DGF©, wrote recently about Dr. Shukla on his 60th birthday; “Professor Dr. Vijay K. S. Shukla celebrated his 60th birthday on 23 March 2008. I am delighted to have this opportunity to show my appreciation of a colleague and friend who is spreading the gospel of lipids, fats and oils around the globe with great success. Vijai was born in 1948 in the holy city of Allahabad, U. P.,India. Having grown up in this city he entered the University of Allahabad to study Chemistry where he specialised in Organic Chemistry. He did his Masters in 1969 and following that, he earned his PhD from the same University in 1973. In fact, he was introduced to the lipid field already in the course of his thesis work. Coming from one of the top Universities in India, he was selected UNESCO fellow to do postdoctoral work first at Charles University in Prague, then in 1975 at the Institute of Neurochemistry in Experimental Life Sciences in Copenhagen, and for one year at the Federal Centre for Lipid Research in Münster, Germany. There he became deeply familiar with lipids, fats and oils that had so much impact on his future professional life. It was also in Münster where we had met first and cooperated. In 1978 he went back to Denmark to join Interferon Laboratories in Hjørring as R&D manager. On the basis of this managerial experience Vijay was subsequently appointed in 1979 as R&D manager by Aarhus Oliefabrik, one of the world’s leading manufacturers of vegetable oils and speciality fats. During the 10 years at this company he built up a strong reputation world-wide for lipid research, particular aspects being analysis, processing and biotechnology. In 1990 he joined Karlshamn Denmark as R&D Director and in 1991 he was ready to start his own company. Vijay founded the “International Food Science Centre” (IFSC), which up-to-date is involved in innovation and acts as extended research centre of the big commercial global players in the areas of lipids, fats and oils. IFSC has become a very successful enterprise with a number of spin-offs set up in several continents. Vijay’s research interests range from physical phenomena to mechanisms of autoxidation, isolation of lipids, spectral phenomena related to lipids (e.g. pulsed NMR), modern analytical methodology, and involvement of essential fatty acids in health and disease such as multiple sclerosis and Batten’s syndrome. Impressively, he has authored a total of over 120 original papers, reviews and book chapters. Moreover, he was and is a much sought-after plenary lecturer at congresses and organizer of short courses; he edited a number of books coming out of these teaching exercises. He has been Associate Editor for INFORM from 1989-97 and still is for J. Am. Oil Chem. Soc., Lipid Technology, and others. In 1996 he received AOCS’ Herbert Dutton Award for his pioneering contributions to the analysis of lipids. Apart from this strong engagement in basic science, his focus has been and is on translation of knowledge gained into industrial applications and commercial success. He has been working hard in the area of confectionary product development and gained special expertise in cocoa butter, milk fat, cocoa butter equivalents and substitutes based on modern concepts of recipe engineering. His accomplishments in this area were acknowledged in 2002 by AOCS by bestowing upon him the prestigious Stephen S. Chang Award; Vijay thanked with an Award lecture, entitled “Chocolate – Friend or Foe”. In another major accomplishment he established in 1996 a refinery in The Netherlands and demonstrated that total oxidation can be arrested during processing and resulting speciality fats of extremely fresh quality can be delivered to customers in the scale of 500-1000 tonnes per shipment. Another achievement is the encapsulation of high amounts of essential PUFA of fish or plant origin combined with natural antioxidant systems to be used as nutritional supplement and as additive in cosmetic formulations. It was pleasing for me to learn that his dedication to basic science and industrial R&D led to Dr. Shukla’s appointment as Adjunct Professor to the Department of Food Science and Human Nutrition of the University of Illinois, Urbana Champaign, USA. As a long-standing member of AOCS he contributed to this Society by serving at top levels in many committees and by sponsoring for 9 years by now the “Young Scientist Award”. Summing up his 8 Presentation of Professor, Dr Vijai K S Shukla

scientific, technical and commercial achievements, and his engagement for the Society, he was elected “AOCS Fellow” in 2005 - well deserved Vijay. And let me add that Vijay convinced me at an AOCS congress in Cincinnati many, many years ago that I must become a member of AOCS. Being also European of Indian background (he became Danish citizen), he had joined also DGF many years ago and through this membership became later member of Euro Fed Lipid as well.We met off and on by visiting and by helping out as organizers and lecturers at various occasions. His relation to and interest for his native India is still strong, for example 8 years ago he founded a subsidiary of IFSC in New Delhi and in 2006 he had a chat even with the President of India discussing technical details about handling of fats and oils. Personally, I remember vividly the fine symposium with top speakers he organized in 2001 near New Delhi to celebrate the 10 Years Jubilee of the very successful IFSC, combined with a lavish treatment of us throughout the conference. So it is my wish and the wish of all those who know Vijay that he continues to thrive in the lipid field we love so much. And, of course, we wish him excellent health in the years to come, as well as the enjoyment of just sitting down and relaxing - at least for a few moments!”

Awards Hindi Rattan Award (2016) Recently, he has been honored by the Government of India with the Hind Rattan Award, one of the highest Indian diasporic awards granted annually to non-resident person of Indian origin by the NRI Welfare Society of India.

AOCS’s Fellows Award (2005) The status of Fellow is awarded to members of the AOCS whose achievements in science entitle them to exceptionally important recognition or to those who have rendered unusually important service to the Society or to the profession. This award recognizes achievements and contributions to the profession, industry and society and encourages future progress in the science.

9 Presentation of Professor, Dr Vijai K S Shukla

AOCS’s Stephen S. Chang Award (2002) This award recognizes a scientist, technologist, or engineer whose distinguished accomplishments in basic research have been used by industries for the improvement or development of products related to lipids.

AOCS’s Herbert J. Dutton Award (1996) The Analytical Division of the AOCS initiated this award to recognize an individual who has made significant contributions to the analyses of fats and oils and related products or whose work has resulted in major advances in the understanding of processes utilized in the fats and oils industry.

AOCS’s Young Scientist Research Award The AOCS Young Scientist Research Award was established to annually recognize a young scientist that has made a significant and substantial research contribution in one of the areas represented by the Divisions of AOCS. The award consists of a plaque, an honorarium, and funding for travel and registration to attend the AOCS Annual Meeting & Expo where the awardee will present a scientific paper relating to the research and development that has merited them the award. Following scientists have been awarded for the last 14 years: 2015 Michael A. Rogers 2011 Raffaele Mezzenga 2007 G. Barcelo-Coblijn 2014 Helen L. Ngo 2010 Edgar J. Acosta 2006 David Compton 2013 Michael A.R. Meier 2009 Ken D. Stark 2005 Ki-Teak Lee 2012 Richard P. Bazinet 2008 Liangli (Lucy) Yu 2004 John N. Coupland

2003 Yeonhwa Park 2002 Anu Hopia 2001 F. Xavier Malcata 2000 A. Marangoni

Research Accomplishments providing global impact in Lipid Research Nutritional significance of lipids in human health and disease Multiple sclerosis and Battens disease: Professor, Dr Vijai K S Shukla has shown essential fatty acid deficiency in multiple sclerosis and Battens disease. These were related with glutathione peroxidase activity and antioxidants requirements in these diseases. Professor, Dr Vijai K S Shukla has also analysed arctic diet in Greenland Eskimos and compared with Danes elucidating some of the mechanism of coronary heart diseases in these population groups. Professor, Dr Vijai K S Shukla successfully demonstrated the presence of selenium in aquatic species which protected polyunsaturated fatty acids due to its antioxidant action. Professor, Dr Vijai K S Shukla's study of erythrocyte glutathione peroxidase activity in comparing Danes and Indian immigrants showed a significant increase in Indian group. This difference was explained based upon selenium and non-selenium enzymes.

Encapsulated oils for corrective nutrition Professor, Dr Vijai K S Shukla developed methodologies to produce highly enriched products for corrective nutrition. He has for last twenty years studied the quality of encapsulated products around the world and showed presence of polymers in fish oil products. These products were highly oxidised and anisidine values were extremely high in fish oil capsules. He has successfully demonstrated that it is possible to produce ultra refined fish oil with extremely low peroxide and anisidine values. This product is under commercial production. Having produced the above mentioned oils it is of utmost importance to keep these oxidation values extremely low therefore he has designed several natural antioxidant systems for general nutrition as well as cosmetic oils. This natural antioxidant system is 50 to 60 times more powerful than existing available antioxidants

Chocolates and confectionery Professor, Dr Vijai K S Shukla has been working in the area of confectionery product development for the last 23 years. He has a special expertise in cocoa butter, milk fat, cocoa butter equivalents and cocoa butter substitutes based on modern concepts of recipe engineering. Professor, Dr Vijai K S Shukla developed NMR technology to study the solid fat contents and triglycerides through HPLC to demonstrate 10 Presentation of Professor, Dr Vijai K S Shukla

the application of these technologies to speciality fats developments. He is a chairman of AOCS NMR group. Professor, Dr Vijai K S Shukla has always applied scientific principles to upgrade or modify existing production to achieve super quality products. Some of his major achievements are as follows: During 1996 Professor, Dr Vijai K S Shukla has established a brand new refinery in Holland and has successfully demonstrated that total oxidation in bulk oils can be completely arrested and speciality fats delivered to the customers will be of extremely fresh quality. These deliveries were in the scale of 5001000 MT per shipment. A proper research approach clearly shows that it is possible to provide uplift to large scale production through extreme care taking with the help of nitrogen as inert gas and stainless steel in the production system. A number of international press articles presented these developments.

Designer oils Professor, Dr Vijai K S Shukla’s recent research focuses on development of highly stable 3 oils for corrective nutrition based upon the technology of internally stabilisation, a process developed by him. This process arrests total oxidation and thus creates highly stable oils for human nutrition.

Novel Introduction of omega-3 in modulating skin metabolism. In human metabolism arachidonic and eicosapentaenoic acids act as a substrate for production of leukotrienes B4 and B5. Leukotrienes B4 are pro-inflammatory together with prostaglandines E2 whereas leukotrienes B5 are antiinflammatory. Modern Western diet has forced omega-6/omega-3 ratio to such a high level whereby we provide excessive substrate of arachidonic acid in promoting the development of leukotrines B4 and thus excessive inflammation. We have successfully produced highly stable omega-3 through our internally stabilisation process whereby it is possible to use these products topically and accelerate the production of leukotrines B5 in reversing inflammation.

Collaboration with Institutes and other Professors Professor Shukla actively collaborates with the following groups: Prof. Henrik Balslev Institutes of Biological Sciences, University of Aarhus Department of Systematic Botany, 68 Nordlandsvej, DK-8240 Risskov, Denmark  Evaluation of Unconventional Oils (from South East Asia and South America Studies of exotic butters for cosmetics) Prof. Fereidoon Shahidi Department of Biochemistry, Memorial University of Newfoundland, St. John's , Newfoundland, Canada  Natural antioxidants Prof. Knud Kragballe Department of Dermatology Marselisborg Hospital, P.P.Oerumsgade 11, DK-8000 Aarhus C, Denmark  Effect of essential fatty acids in Human skin and diseases Prof. William E. Artz University of Illinois, Urbana-Champaign, Dept of Food Science & Human Nutrition, Urbana, IL61801, USA  Evaluation of Unconventional oils through Modern Analytical Technology

11 Presentation of Professor, Dr Vijai K S Shukla

List of Publications 1970 -1980 1. "Engineering Chemistry". For Technical University Students. 1972. 2. Sharma, J. P.; Awasthy, A. K.; Shukla, V. K. S.: Micro determination of olefinic unsaturation using bromine monochloride in acetic acid medium. Mikrochimica Acta, 522, 1972. 3. Shukla, V. K. S.; Pande, U. C.; Sharma, J. P.: Micro determination of olefinic unsaturation. Reaction of N-Bromosuccinimide with olefins in polar medium. Z. Anal. Chem. 260, 359, 1972. 4. Shukla, V. K. S.; Shukla, S.; Sharma, J. P.: Volumetric micro determination of sulphonamides. Z. Anal. Chem. 265, 352, 1973. 5. "Decade Chemistry", Indian Science Congress Association, 1973. 6. molybdic acid complex. Z. Anal. Chem. 276, 300, 1975. 7. Shukla, V. K. S.; Shukla, S.: Micro determination of histamine and serotonin drugs using bromine monochloride in water-acetic acid medium. Microchemical Journal, 21, 242, 1976. 8. Sharma, J. P.; Shukla, V. K. S.; Dubey, A. K.: Micro determination of pyrrole derivatives with NBromosuccinimide in acetic acid medium. Analyst, 101, 867, 1976. 9. Shukla, V. K. S.; Dubey, A. K.; Sharma, J. P.: Volumetric micro determination of hydrazines and hydrazides. Analytical Letters, 9, 975, 1976. 10. Sharma, J. P.; Shukla, V. K. S.; Dubey, A. K.: Spectrophotometric determination of pyrrole derivatives. Talanta, 23, 841, 1976. 11. Shukla, V. K. S.; Shukla, S.: Micro determination of furfural using bromine monochloride. Bull. Chem. Soc. Japan, 50, 559, 1977. 12. Sharma, J. P.; Shukla, V. K. S.; Dubey, A. K.: Micro determination of aromatic amines and phenols using bromine monochloride in acetic acid medium. Mikrochimica Acta, 357, 1977. 13. Sharma, J. P.; Shukla, V. K. S.; Dubey, A. K.: Micro determination of pyrrole derivaties using bromine monochloride in acetic acid medium. Chemical & Pharmaceutical Bulletin, 25, 1493, 1977. 14. Shukla, V. K. S.: Micro determination of thiourea, allylthiourea, phenyl urea using bromine monochloride in water-acetic acid medium. Analyst, 102, 691, 1977. 15. Shukla, V. K. S.; Clausen, J.: Micro determination of ascorbic acid using bromine monochloride in water-acetic acid medium. Microchemical Journal, 22 (4), 475, 1977. 16. Shukla, V. K. S.; Jensen, E.; Clausen, J.: Erythrocyte glutathione peroxidase deficiency in Multiple Sclerosis. Acta Neurologica Scandinavia, 56, 542, 1977. 17. Shukla, V. K. S.; Sharma, J. P.: Kinetics and mechanism of Bromination of Crotonic acid by NBromosuccinimide. Monatshefte für Chemie, 109, 451, 1978. 18. Shukla, V. K. S.; Clausen, J.: Linoleate and fatty acids pattern of serum lipids in Multiple Sclerosis. Acta Neurolog. Scand. 57, 270, 1978. 19. Jensen, E; Shukla, V. K. S.; Nielsen, G.; Clausen, J.: Biochemical abnormalities in Batten's syndrome. Scand. J. Clin. Lab. Invest. 38, 309, 1978. 20. Shukla, V. K. S.; Jensen, E.; Clausen, J.: Serum fatty acids and peroxidase abnormalities in Batten's disease. Res. Exptl. Med. 173, 27, 1978. 21. Shukla, V. K. S.; Srivastava, K. C.: A simple procedure for the Chromatographic isolation and determination of prostaglandins from human seminal plasma. Z. Anal. Chem. 293, 45, 1978. 22. Shukla, V. K. S.; Srivastava, K. C.: Argentation thin layer chromatography of polyunsaturated fatty acid methyl esters. J. High Res. Chromato. & Chromatog. Commun. 215, Oct. 1978. 23. Shukla, V. K. S.; Srivastava, K. C.: Erythrocyte glutathione peroxidase and serum lipid pattern: A comparison between Indian immigrants and Danes. Z. Ernarungswissenschaft, 17, 240, 1978. 24. Shukla, V. K. S.; Abdel-Moety, E. M.; Larsen, E.; Egsgaard, H.: Identification of cyclopentenyl fatty acids by gas liquid chromatography and mass spectrometry. Chem. Phys. Lipids. 23, 285, 1979. 25. Shukla, V. K. S.; Kokate, C. K.; Srivastava, K. C.: Spectrophotometric determination of ascorbic acid. Michrochem. J. 24, 124, 1979. 26. Shukla, V. K. S.; Paulose, M. M.: The surface lipids of Hydnocarpus Wightiana leaves. Chem. Phys. Lipids, 25, 1, 1979. 12 Presentation of Professor, Dr Vijai K S Shukla

27. Shukla, V. K. S.; Clausen, J.; Egsgaard, H.; Larsen, E.: The content of fat and polyenoic acids in the major food sources of the arctic diet. Localization of double bonds in fatty acids by means of mass spectrometry of fatty acid pyrolidides. Fette, Seifen, Anstrich. 82, 193, 1980.

1981 -1990 28. Shukla, V. K. S.: Studies on the crystallization behaviour of the cocoa butter equivalents by pulsed NMR employing various tempering modes. Food R. A. Leatherhead reports, 24 May 1983. 29. Shukla, V. K. S.; Schiøtz Nielsen, W.: A simple and direct procedure for the evaluation of triglyceride composition of cocoa butters by high performance liquid chromatography - A comparison with the existing TLC-GC method. Fette, Seifen, Anstrich. 85, 274, 1983. 30. Shukla, V. K. S.: Studies on the crystallization behaviour of the cocoa butter equivalents by pulsed Nuclear Magnetic Resonance - Part I. Fette, Seifen, Anstrich. 85, 467, 1983. 31. Shukla, V. K. S.; Spener, F.: High performance liquid chromatography of triglycerides of Flacourtiaceae seed oils containing cyclopentenyl fatty acids (chaulmoogric oils). J. Chromatog. 348, 441, 1985. 32. Shukla, V. K. S.: Recent applications of the high performance liquid chromatography to oils and fats analysis. Proceedings of the 13th Scand. Symp. on Lipids. Reykjavik, Iceland, 1985. 33. Shukla, V. K. S.: Applications of the high performance liquid chromatography to oils and fats analysis. J. Am. Oil Chem. Soc. 62, 610, 1985. 34. Shukla, V. K. S.: High speed liquid chromatography as applied to oils and fats analysis. J. Am. Oil Chem. Soc. 63, 416, 1986. 35. Shukla, V. K. S.; Nielsen, S.: Application of high performance liquid chromatography for the evaluation of unconventional oils, Proceedings of the 14th Scand. Symp. on Lipids. Mora, Sweden, June 1987. 36. Shukla, V. K. S.: Quantitative determination of oligosaccharides in defatted soybean products by high speed liquid chromatography. Fette, Seifen, Anstrich. 89, 75, 1987. 37. Shukla, V. K. S.; Andersen, A. B.: High speed liquid chromatography as applied to the analysis of glucosinolates in rapeseed products. HPLC, 1987. 38. Shukla, V. K. S.: Studies on the crystallization behavior of the confectionery fats by pulse Nuclear Magnetic Resonance employing various tempering modes. J. Am. Oil Chem. Soc. 64, 658, 1987. 39. Fogh, K.; Kragballe, K.; Larsen, E.; Egsgaard, H.; Shukla, V. K. S.: Mass spectrometry of underivatized 15-hydroxy-eicosatetraenoic acid and 15-hydroxy-eicosapentaenoic acid. Biomedical and Environmental Mass Spectrometry. 17, 459, 1988. 40. Tolboe, O.; Hansen, I.R.; Shukla, V.K.S.: Extraction of Oil from Evening Primrose Seed. Proceedings of International Symposium on Supercritical Fluids, Nice, France. Oct. 1988. 41. "Recent advances in the high performance liquid chromatography of lipids". 41.1.1. Progress in Lipid Research, 1988. 42. "Confectionery fats". Elsevier's Development Series, 1988. 43. Christie, W. W.; Brechany, E. Y.; Shukla, V. K. S.: Analysis of seed oils containing cyclopentenyl fatty acids by combined chromatographic procedures. Lipids, 24, 116, 1989. 44. Shukla, V. K. S.: Application of high performance liquid chromatography for evaluation of lipid structures. J. Dispersion Science and Technology, 10, 581, 1989. 45. Shukla, V.K.S.; Nielsen, I.C.: Diversity of Minor Tropical Tree Crops and Their Importance for the Industrialized World. Tropical Forests. Academic Press Limited. 1989. 46. Kragballe, K.; Shukla, V. K. S.: Polyumættede fedtsyrepræparater på det danske marked. Ugeskrift for læger. 152, 894, 1990. 47. Shukla, V. K. S.: Dietary essential fatty acids and antioxidants. Lipid Technology, 2, Jan 1990. 48. "Milk fat in sugar and chocolate confectionery". Elsevier Applied Science Publishers Limited, 1990. 49. Shukla, V. K. S.: Rancidity in health food oils. British Food Manufacturing Industries Research Association. Symposium Proceedings. 45, May 1990.

1991 -2000 50. "Application of NMR Spectrometry: Pulsed NMR". Analyses of Fats, Oils and Lipoproteins. AOCS. 1991. 51. "Application of High Performance Liquid Chromatography to Lipid Separation and Analysis: Lipid Derivatives". Analyses of Fats, Oils and Lipoproteins. AOCS. 1991.

13 Presentation of Professor, Dr Vijai K S Shukla

52. "Application of High Performance Liquid Chromatography of Triglycerides to Lipid Separation and Analysis: Neutral Lipids". Analyses of Fats, Oils and Lipoproteins. AOCS. 1991. 53. Shukla, V. K. S.; Perkins, E. G.: The presence of oxidative polymeric materials in encapsulated fish oils. Lipids. Vol. 26, No. 1, 1991. 54. Shukla, V.K.S.: Applications of Pulsed NMR Techniques for Food Analysis. IFSC 1991. 55. Shukla, V.K.S.: Antioxidants in Foods and the Treatment of Human Diseases. IFSC 1991. 56. Shukla, V.K.S.; Gunstone, F.D.: Oils and Fats in the Nineties. IFSC 1992. 57. Shukla, V.K.S.; Diplock, A.T.; Gutteridge, J.M.C.: Antioxidants, Free Radicals and Polyunsaturated Fatty Acids in Biology and Medicine. IFSC 1993. 58. Shukla, V.K.S.; Blicher-Mathiesen, U.: Studies in Evaluation of Unconventional Oils from Southeast Asia. Fat Sci. Tehcnol., 95. Jahrgang, Nr. 10, 1993. 59. MSK Syed Rahmatullah, Shukla, V -Linolenic Acid from Evening Primrose Oil and Borage Oil via Lipase-Catalyzed Hydrolysis. JAOCS. Vol. 71, no. 6 (June 1994). 60. -Linolenic Acid Concentrates from Borage and Evening Primrose Oil Fatty Acids via Lipase-Catalyzed Esterification. JAOCS. Vol. 71, no. 6 (June 1994). 61. "Present and Future Outlook of the World Fats and Oil Supplies". Technological Advances in Improved and Alternative Sources of Lipids. B.S. Kamel and Y. Kakuda. Blackie Academic & Professional. 1994. 62. "Milk fat in sugar and chocolate confectionery". Fats in Food products. D.P.J. Moran and K.K. Rajah, Blackie Academic & Professional. 1994. 63. "Oil Processing in the 21st Century". European Food and Drink Directory 1994/95. 1994. 64. "Cocoa Butter properties and Quality". Lipid Technology. 1995. 65. "Thin-Layer Chromatography of Lipids". New Trends in Lipid and Lipoproten Analyses. AOCS Press. 1995. 66. "High-Performance Liquid Chromatography: Normal-Phase, Reverse-Phase Detection Methodology". New Trends in Lipid and Lipoproten Analyses. AOCS Press. 1995. 67. "The Role of Dietary Fats and Oils". Fats, Oleochemicals and Surfactants. Challenges in the 21st Century. V.V.S. Mani and A.D. Shitole. Oxford & IBH Publishing Co. PVT. Ltd. OTAI , 1997. 68. "Milkfat and Its applications". The World of Ingredients. The Journal of the Practicing Food Technologist. January-February 1995. 69. Shukla, V.K.S.; Gunstone, F.D.: "NMR of Lipids". Annual Reports on NMR Spectroscopy. Volume 31. Academic Press. 1995. 70. Shukla, V.K.S.; Jensen, Ole Holm: Fatty Acid Composition and Tocopherol Content of Amazonian Palm Oils. Journ. of Food Lipids 3, 1996. 71. Shukla, V.K.S.; Shahidi, F; Wanasundara, P.K.J.P.D.: Endogenous Antioxidants from Oilseeds and Edible Oils, Food Rev. Int. 13 (2), 225-292, 1997. 72. Shukla, V.K.S.; Shahidi, F.: Non-triacylglycerol Constituents of Fats and oils. INFORM. Vol. 7, no. 11 1227-1232. November Issue. 1996. 73. Shukla, V.K.S.; Shahidi, F; Wanasundara, Udaya N.; He, Y.: “Marine Lipids and Their Stabilization with Green Tea and Catechins”. Flavor and Lipid Chemistry of Seafoods, 1997. ACS Washington. 74. Shukla, V.K.S.; Shahidi, F.; Wanasundara P.K.J.P.D.: “Natural Antioxidants from Oilseeds”. Natural Antioxidants, Chemistry, Health Effects, and Applications. 1997. AOCS Press. 75. Shukla, V.K.S.: ”Chocolate – The Chemistry of Pleasure”. INFORM, Vol. 8, no. 2 (February 1997). 76. Shukla, V.K.S.: ”Description of the IFSC minideodorizer”. INFORM, Vol. 8, no. 11 (November 1997). 77. Shukla, V.K.S.; Kragballe K: ”Exotic Butters as Cosmetic Lipids”. INFORM, Vol. no. 5 (May 1998). 78. Shukla, V.K.S.; Perkins, E.G.: Rancidity in Health Food Oils. INFORM, Vol. 9, (October 1998). 79. Shukla, V.K.S.; Goudappel, G.-J.; Gribnau, M.C.M; van Duynhoven, Solid Fat Content Determination by NMR. J. INFORM, Vol. 10 (May 1999).

14 Presentation of Professor, Dr Vijai K S Shukla

2001 - 2010 80. Shukla, V.K.S.; Organic foods: present and future developments INFORM, Vol. No. 12 (May 2001). 81. Shukla, V.K.S.; Bhattacharya, K: Mango Butter in Cosmetic Formulations, Cosmetics & Toiletries, Vol. 117, No. 6 (June 2002). 82. Shukla, V.K.S.; Chocolate – A Food from the Past with a Future. INFORM, Vol. No. 13 (October 2002). 83. Shukla, V.K.S.; Dutta, P.C.; Artz, W.E.: Camelina Oil and its Unusual Cholesterol Content. JAOCS, Vol. 79, no. 10 (October 2002). 84. Shukla, V.K.S.; Bhattacharya, K.; Nutridan bakes a recipe for health. Oils and Fats International, May 2003. 85. Shukla, V.K.S.. A designer oil for better health. INFORM, Vol. No. 14 (June 2003). 86. Shukla, V.K.S., Bhattacharya, K.. Extending the shelf life of cosmetic products through novel stabilisation of exotic butters and oils, SÖFW-Journal Seifen, Öle, Fette, Wachse, 129, Jahrgang 92003. 87. Shukla, V.K.S., Bhattacharya, K. Enhancing the Stability Of Exotic Butters & Oils, Happi Magazine (Household and Personal Products Industry), December 2003. 88. Shukla, V.K.S., Bhattacharya, K. The magic of Rosemary, Oils & Fats International, January 2004. 89. Nielsen, Henning; Shukla, Vijai K.S.: In situ solid Phase Extraction of Lipids from Spray-dried Egg Yolk by Ethanol with Subsequent Removal of Triacylglycerols by Cold Temperature Crystallization. Swiss Society of Food Science and Technology. Elsevier Ltd. 2004 90. Shukla, Vijai K.S.: Designing Natural Cosmetics through the Dynamics of Naturally Derived Lipids, INFORM, Vol. 15 (4) (April 2004). 91. Shukla, Vijai K.S.; Bhattacharya, Kaustuv: Enhancing the Stability of Natural Oils and Butters with Rosemary Extracts, Cosmetics & Toiletries, Vol. 119, No. 5/May 2004. 92. Shukla, Vijai K.S.: The challenges of skin care, INFORM, Vol. 15 (5) (May 2004). 93. Shukla, Vijai K.S.; Bhattacharya, Kaustuv: Correcting omega-6/omega-3 balance in human diet by internally stabilised designer oil, Agro Food industry hi-tech, Tekno Scienze, Anno 15, May/June 2004. 94. Shukla, Vijai K.S.; Bhattacharya, Kaustuv: Novel introduction of omega-3 oils for enhancing the value of cosmeceuticals. NutraCos, Anno 3 – N. 3, B5 srl, May/June 2004, 95. Shukla, Vijai K.S.; Bhattacharya, Kaustuv: Nutridan, a vegetable-based source of omega-3. bake & take, The Journal of the National Association of Master Bakers, Dec 2004/Jan 2005. 96. Shukla, Vijai K.S.: New Horizons in the Development of Natural Oils and Butters as cosmetic Ingredients – Novel Introduction of Stabilized Omega-3 in Cosmeceuticals. T4 Group, UK. 2005. 97. Shukla, Vijai K.S.: The skinny on fats better functionality equals better products. Organic Processing Magazine CA, USA, Oct-Dec 2007, Vol 4, No 4 98. Shukla, Vijai K.S.: Innovative organic lipids in cosmeceuticals, Inform, Vol 19 (4), April 2008 99. Shukla, Vijai K.S.: Organic health food for rejuvenated bio skincare formulations emplying the power of chemoprenters. T4 Group UK, 2008. 100. Shukla, Vijai K.S.: Innovative Organic Lipids in Filtering the Chemistry in Cosmeceuticals, Cosmetic Science Technology, 2009 101. Shukla, Vijai K.S.: Natural oils & butters in cosmetics, book chapter “the Chemistry and manufacture nd of cosmetics, Vol. 3” Ingredients 2 edition 102. Shukla, Vijai K.S., Le Poole, Hendrik A.C.: Review of Some Unconventional Tree Seed Oils from Africa for Application in Cosmetics, Cosmetic Science Technology, 2010 103. Shukla, Vijai K.S., Nielsen, Søren: Novel introduction of Spice and Fruit Butters and Oils in Cosmetic Applications, 2012. 105. Shukla, Vijai K.S., Nielsen, Søren: Enhancing the Value of Cosmeceuticals Through Internally Stabilised Spice Formulations in Cosmetic Applications, 2013. 106. Studies in the evaluation of unconventional oils from Burkina Faso, Part 1: Page 31- Cosmetic Applications, 2014 107. Shukla, Vijai K.S., Nielsen, Søren: Studies in the evaluation of unconventional oils from Burkina Faso, rich in Linoleic acid (C18:2 n-6) or other unusual fatty acids, Part 2: Cosmetic Applications 2015.

15 Presentation of Professor, Dr Vijai K S Shukla

2011 108. Shukla, Vijai K.S., Nielsen, Søren: Novel Introduction of Spise and Fruit Butters and Oils in Cosmetic Applications, Cosmetic Science Technology 2012 109. Shukla, Vijai K.S., Nielsen, Søren: Enhancing the Value of Cosmeceuticals Through Internally Stabilised Spice Formulations, Cosmetic Science Technology 2013 110. Shukla, Vijai K.S., Nielsen, Søren: Studies in the Evaluation of Unconventional Oils from Burkina Faso – Part One: Rich in Oleic Acid (C18:1 n-9), Cosmetic Science Technology 2014

16 Presentation of Professor, Dr Vijai K S Shukla