Appendix A Laboratory Analytical Reports
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 REPORT DATE
6/27/2008
EARTH TECH - CONCORD 300 BAKER AVE., SUITE 290 CONCORD, MA 01742 ATTN: ELISSA BROWN
CONTRACT NUMBER: PURCHASE ORDER NUMBER: PROJECT NUMBER: ANALYTICAL SUMMARY LIMS BAT #:
LIMT-17022
JOB NUMBER:
63728
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report. Results are based on samples as submitted to the laboratory and relate only to the items collected and tested.
PROJECT LOCATION:
FIELD SAMPLE #
MBTA-READVILLE
LAB ID
MATRIX
SAMPLE DESCRIPTION
TEST
Text28: 0637(3.0-6.0)
08B22605
SOIL
Not Specified
as (mg/kg)dw icp
0637(3.0-6.0) Text28:
08B22605
SOIL
Not Specified
eph - solid 04
0637(3.0-6.0) Text28:
08B22605
SOIL
Not Specified
pb (mg/kg)dw icp
0637(3.0-6.0) Text28:
08B22605
SOIL
Not Specified
solids (percent)
0637(3.0-6.0) Text28:
08B22613
SOIL
Not Specified
tclp - lead icp
0692(0.5-2.0) Text28:
08B22603
SOIL
Not Specified
as (mg/kg)dw icp
0692(0.5-2.0) Text28:
08B22603
SOIL
Not Specified
eph - solid 04
0692(0.5-2.0) Text28:
08B22603
SOIL
Not Specified
pb (mg/kg)dw icp
0692(0.5-2.0) Text28:
08B22603
SOIL
Not Specified
solids (percent)
0692(0.5-2.0) Text28:
08B22611
SOIL
Not Specified
tclp - lead icp
0694(0.5-3.0) Text28:
08B22606
SOIL
Not Specified
as (mg/kg)dw icp
0694(0.5-3.0) Text28:
08B22606
SOIL
Not Specified
eph - solid 04
0694(0.5-3.0) Text28:
08B22606
SOIL
Not Specified
pb (mg/kg)dw icp
0694(0.5-3.0) Text28:
08B22606
SOIL
Not Specified
solids (percent)
0694(0.5-3.0) Text28:
08B22614
SOIL
Not Specified
tclp - lead icp
0906(0.0-0.5) Text28:
08B22604
SOIL
Not Specified
as (mg/kg)dw icp
0906(0.0-0.5) Text28:
08B22604
SOIL
Not Specified
eph - solid 04
0906(0.0-0.5) Text28:
08B22604
SOIL
Not Specified
pb (mg/kg)dw icp
0906(0.0-0.5) Text28:
08B22604
SOIL
Not Specified
solids (percent)
0906(0.0-0.5) Text28:
08B22612
SOIL
Not Specified
tclp - lead icp
1016(0-0.5) Text28:
08B22599
SOIL
Not Specified
as (mg/kg)dw icp
1016(0-0.5) Text28:
08B22599
SOIL
Not Specified
eph - solid 04
1016(0-0.5) Text28:
08B22599
SOIL
Not Specified
pb (mg/kg)dw icp
1016(0-0.5) Text28:
08B22599
SOIL
Not Specified
solids (percent)
1016(0-0.5) Text28:
08B22607
SOIL
Not Specified
tclp - lead icp
1020(0.5-3.0) Text28:
08B22601
SOIL
Not Specified
as (mg/kg)dw icp
1020(0.5-3.0) Text28:
08B22601
SOIL
Not Specified
eph - solid 04
1020(0.5-3.0) Text28:
08B22601
SOIL
Not Specified
pb (mg/kg)dw icp
1020(0.5-3.0) Text28:
08B22601
SOIL
Not Specified
solids (percent)
1020(0.5-3.0) Text28:
08B22609
SOIL
Not Specified
tclp - lead icp
1078(3.0-6.0) Text28:
08B22602
SOIL
Not Specified
as (mg/kg)dw icp
1078(3.0-6.0) Text28:
08B22602
SOIL
Not Specified
eph - solid 04
1078(3.0-6.0) Text28:
08B22602
SOIL
Not Specified
pb (mg/kg)dw icp
1078(3.0-6.0) Text28:
08B22602
SOIL
Not Specified
solids (percent)
1078(3.0-6.0) Text28:
08B22610
SOIL
Not Specified
tclp - lead icp
1130(0-0.5) Text28:
08B22600
SOIL
Not Specified
as (mg/kg)dw icp
1130(0-0.5) Text28:
08B22600
SOIL
Not Specified
eph - solid 04
Subcontract Lab (if any) Cert. Nos.
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 REPORT DATE EARTH TECH - CONCORD 300 BAKER AVE., SUITE 290 CONCORD, MA 01742 ATTN: ELISSA BROWN
CONTRACT NUMBER: PURCHASE ORDER NUMBER: PROJECT NUMBER: ANALYTICAL SUMMARY LIMS BAT #:
LIMT-17022
JOB NUMBER:
63728
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report. Results are based on samples as submitted to the laboratory and relate only to the items collected and tested. Text28: 1130(0-0.5) 08B22600 SOIL Not Specified pb (mg/kg)dw icp 1130(0-0.5) Text28:
08B22600
SOIL
Not Specified
solids (percent)
1130(0-0.5) Text28:
08B22608
SOIL
Not Specified
tclp - lead icp
6/27/2008
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 REPORT DATE EARTH TECH - CONCORD 300 BAKER AVE., SUITE 290 CONCORD, MA 01742 ATTN: ELISSA BROWN
CONTRACT NUMBER: PURCHASE ORDER NUMBER: PROJECT NUMBER: ANALYTICAL SUMMARY LIMS BAT #:
LIMT-17022
JOB NUMBER:
63728
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report. Results are based on samples as submitted to the laboratory and relate only to the items collected and tested.
Comments : LIMS BATCH NO. : LIMT-17022 CASE NARRATIVE SUMMARY Recommended sample holding times were not exceeded for all samples unless listed below: None Exceeded All samples for the method(s) listed were received preserved properly in the proper containers at 4°C +/- 2 degrees as specified on the chain-of-custody form unless listed below: All properly preserved There are no analytical issues which affect the usability of the data. DETAILED CASE NARRATIVE
EXTRACTABLE PETROLEUM HYDROCARBONS (EPH) MADEP-EPH-04-1.1 ADDITIONAL DETAILS Solid samples, if any, in the batch were extracted by the following method: Microwave: SW846 3546 SPE cartridge contamination with non-petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C11-C22 aromatic range fraction in all samples in the batch. Target compounds are subtracted from the C11-C22 aromatic range but not from the unadjusted C11-C22 aromatic range. No significant modifications were made to the method. All EPH samples were analyzed undiluted unless specified below: Sample Dilution(s) 08B22603 x5 and undilute 08B22604 x10 08B22606 x5 and undilute
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations. AIHA accreditations only apply to NIOSH methods and Environmental Lead Analyses. AIHA 100033 AIHA ELLAP (LEAD) 100033 NORTH CAROLINA CERT. # 652 MASSACHUSETTS MA0100
NEW HAMPSHIRE NELAP 2516
NEW JERSEY NELAP NJ MA007 (AIR)
CONNECTICUT PH-0567
VERMONT DOH (LEAD) No. LL015036
FLORIDA DOH E871027 (AIR)
NEW YORK ELAP/NELAP 10899
RHODE ISLAND (LIC. No. 112)
6/27/2008
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 1 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 0637(3.0-6.0) Sample ID :
08B22605
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Results
Units
Date
Analyst
RL
Analyzed Arsenic
mg/kg dry wt
25.8
SPEC Limit Lo
06/25/08
OP
3.06
Date
Analyst
RL
P/ F
Hi
Field Sample # : 0692(0.5-2.0) Sample ID :
08B22603
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Analyzed Arsenic
mg/kg dry wt
69.5
SPEC Limit Lo
06/25/08
OP
3.09
Date
Analyst
RL
P/ F
Hi
Field Sample # : 0694(0.5-3.0) Sample ID :
08B22606
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Analyzed Arsenic
mg/kg dry wt
61.6
SPEC Limit Lo
06/25/08
OP
3.26
Date
Analyst
RL
P/ F
Hi
Field Sample # : 0906(0.0-0.5) Sample ID :
08B22604
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Analyzed Arsenic
mg/kg dry wt
20.0
SPEC Limit Lo
06/25/08
OP
2.76
P/ F
Hi
Field Sample # : 1016(0-0.5) Sample ID :
08B22599
Sample Matrix:
SOIL
‡Sampled : 6/18/2008 Not Specified
Arsenic
Units
Results
Date Analyzed
Analyst
RL
mg/kg dry wt
12.2
06/25/08
OP
3.07
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
SPEC Limit Lo Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 2 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 1020(0.5-3.0) Sample ID :
08B22601
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Results
Units
Date
Analyst
RL
Analyzed Arsenic
mg/kg dry wt
13.1
SPEC Limit Lo
06/25/08
OP
2.66
Date
Analyst
RL
P/ F
Hi
Field Sample # : 1078(3.0-6.0) Sample ID :
08B22602
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Units
Results
Analyzed Arsenic
mg/kg dry wt
5.21
SPEC Limit Lo
06/25/08
OP
2.57
Date
Analyst
RL
P/ F
Hi
Field Sample # : 1130(0-0.5) Sample ID :
08B22600
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Units
Results
Analyzed Arsenic
mg/kg dry wt
14.5
06/25/08
SPEC Limit Lo
OP
2.57
Analytical Method: SW846 3050/6010 SAMPLES ARE DIGESTED WITH NITRIC ACID AND THEN ANALYZED BY INDUCTIVELY COUPLED PLASMA EMISSION SPECTROSCOPY.
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 3 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 0637(3.0-6.0) Sample ID :
08B22605
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Date
Analyst
RL
Analyzed
Lo
C9-C18 Aliphatics
mg/kg dry wt
50.2
06/25/08
CJM
36.7
C19-C36 Aliphatics
mg/kg dry wt
56.8
06/25/08
CJM
36.7
Unadjusted C11-C22 Aromatics
mg/kg dry wt
258
06/25/08
CJM
36.7
C11-C22 Aromatics
mg/kg dry wt
252
06/25/08
CJM
36.7
Acenaphthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Acenaphthylene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
Anthracene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
Benzo(a)anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(a)pyrene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(b)fluoranthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(g,h,i)perylene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(k)fluoranthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Chrysene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Dibenzo(a,h)anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Fluoranthene
mg/kg dry wt
0.5
06/25/08
CJM
0.2
Fluorene
mg/kg dry wt
1.0
06/25/08
CJM
0.2
Indeno(1,2,3-cd)pyrene
mg/kg dry wt
ND
06/25/08
CJM
0.2
2-Methylnaphthalene
mg/kg dry wt
0.8
06/25/08
CJM
0.2
Naphthalene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
Phenanthrene
mg/kg dry wt
1.4
06/25/08
CJM
0.2
Pyrene
mg/kg dry wt
1.2
06/25/08
CJM
0.2
6/23/2008
06/25/08
CJM
Date Extracted EPH Solid
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
SPEC Limit Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 4 of 25
CONCORD, MA 01742
Purchase Order No.:
Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 0637(3.0-6.0) Analytical Method: MADEP-EPH-04-1 SAMPLES ARE EXTRACTED WITH METHYLENE CHLORIDE AND ACETONE BY PRESSURIZED FLUID EXTRACTION (SW846 3545) OR MICROWAVE (SW846 3546), EXCHANGED INTO HEXANE AND CONCENTRATED. ALIPHATIC AND AROMATIC FRACTIONS ARE SEPARATED. ANALYSIS IS BY GAS CHROMATOGRAPHY WITH FLAME IONIZATION DETECTION. PAH AND C11-C22 AROMATICS ARE DETERMINED IN THE METHYLENE CHLORIDE FRACTION. C9-C18 AND C19-C36 ALIPHATICS ARE DETERMINED IN THE HEXANE FRACTION. TARGET COMPOUND CONTRIBUTIONS ARE SUBTRACTED FROM THE SUMMED AROMATIC RANGE, BUT NOT FROM THE UNADJUSTED C11-C22 AROMATIC RANGE.
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 5 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 0692(0.5-2.0) Sample ID :
08B22603
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Date
Analyst
RL
Analyzed
Lo
C9-C18 Aliphatics
mg/kg dry wt
83.8
06/25/08
CJM
37.1
C19-C36 Aliphatics
mg/kg dry wt
644
06/25/08
CJM
37.1
Unadjusted C11-C22 Aromatics
mg/kg dry wt
197
06/25/08
CJM
37.1
C11-C22 Aromatics
mg/kg dry wt
190
06/25/08
CJM
37.1
Acenaphthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Acenaphthylene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Anthracene
mg/kg dry wt
0.2
06/25/08
CJM
0.2
Benzo(a)anthracene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
Benzo(a)pyrene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(b)fluoranthene
mg/kg dry wt
0.3
06/25/08
CJM
0.2
Benzo(g,h,i)perylene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(k)fluoranthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Chrysene
mg/kg dry wt
0.5
06/25/08
CJM
0.2
Dibenzo(a,h)anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Fluoranthene
mg/kg dry wt
1.0
06/25/08
CJM
0.2
Fluorene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
Indeno(1,2,3-cd)pyrene
mg/kg dry wt
ND
06/25/08
CJM
0.2
2-Methylnaphthalene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
Naphthalene
mg/kg dry wt
0.7
06/25/08
CJM
0.2
Phenanthrene
mg/kg dry wt
1.2
06/25/08
CJM
0.2
Pyrene
mg/kg dry wt
1.0
06/25/08
CJM
0.2
6/23/2008
06/25/08
CJM
Date Extracted EPH Solid
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
SPEC Limit Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 6 of 25
CONCORD, MA 01742
Purchase Order No.:
Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 0692(0.5-2.0) Analytical Method: MADEP-EPH-04-1 SAMPLES ARE EXTRACTED WITH METHYLENE CHLORIDE AND ACETONE BY PRESSURIZED FLUID EXTRACTION (SW846 3545) OR MICROWAVE (SW846 3546), EXCHANGED INTO HEXANE AND CONCENTRATED. ALIPHATIC AND AROMATIC FRACTIONS ARE SEPARATED. ANALYSIS IS BY GAS CHROMATOGRAPHY WITH FLAME IONIZATION DETECTION. PAH AND C11-C22 AROMATICS ARE DETERMINED IN THE METHYLENE CHLORIDE FRACTION. C9-C18 AND C19-C36 ALIPHATICS ARE DETERMINED IN THE HEXANE FRACTION. TARGET COMPOUND CONTRIBUTIONS ARE SUBTRACTED FROM THE SUMMED AROMATIC RANGE, BUT NOT FROM THE UNADJUSTED C11-C22 AROMATIC RANGE.
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 7 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 0694(0.5-3.0) Sample ID :
08B22606
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Date
Analyst
RL
Analyzed
Lo
C9-C18 Aliphatics
mg/kg dry wt
232
06/25/08
CJM
39.2
C19-C36 Aliphatics
mg/kg dry wt
610
06/25/08
CJM
39.2
Unadjusted C11-C22 Aromatics
mg/kg dry wt
418
06/25/08
CJM
39.2
C11-C22 Aromatics
mg/kg dry wt
390
06/25/08
CJM
39.2
Acenaphthene
mg/kg dry wt
0.9
06/25/08
CJM
0.2
Acenaphthylene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
Anthracene
mg/kg dry wt
0.8
06/25/08
CJM
0.2
Benzo(a)anthracene
mg/kg dry wt
0.9
06/25/08
CJM
0.2
Benzo(a)pyrene
mg/kg dry wt
0.7
06/25/08
CJM
0.2
Benzo(b)fluoranthene
mg/kg dry wt
0.9
06/25/08
CJM
0.2
Benzo(g,h,i)perylene
mg/kg dry wt
0.6
06/25/08
CJM
0.2
Benzo(k)fluoranthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Chrysene
mg/kg dry wt
1.3
06/25/08
CJM
0.2
Dibenzo(a,h)anthracene
mg/kg dry wt
0.3
06/25/08
CJM
0.2
Fluoranthene
mg/kg dry wt
4.0
06/25/08
CJM
0.2
Fluorene
mg/kg dry wt
1.8
06/25/08
CJM
0.2
Indeno(1,2,3-cd)pyrene
mg/kg dry wt
0.6
06/25/08
CJM
0.2
2-Methylnaphthalene
mg/kg dry wt
1.5
06/25/08
CJM
0.2
Naphthalene
mg/kg dry wt
2.4
06/25/08
CJM
0.2
Phenanthrene
mg/kg dry wt
6.6
06/25/08
CJM
0.2
Pyrene
mg/kg dry wt
4.9
06/25/08
CJM
0.2
6/23/2008
06/25/08
CJM
Date Extracted EPH Solid
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
SPEC Limit Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 8 of 25
CONCORD, MA 01742
Purchase Order No.:
Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 0694(0.5-3.0) Analytical Method: MADEP-EPH-04-1 SAMPLES ARE EXTRACTED WITH METHYLENE CHLORIDE AND ACETONE BY PRESSURIZED FLUID EXTRACTION (SW846 3545) OR MICROWAVE (SW846 3546), EXCHANGED INTO HEXANE AND CONCENTRATED. ALIPHATIC AND AROMATIC FRACTIONS ARE SEPARATED. ANALYSIS IS BY GAS CHROMATOGRAPHY WITH FLAME IONIZATION DETECTION. PAH AND C11-C22 AROMATICS ARE DETERMINED IN THE METHYLENE CHLORIDE FRACTION. C9-C18 AND C19-C36 ALIPHATICS ARE DETERMINED IN THE HEXANE FRACTION. TARGET COMPOUND CONTRIBUTIONS ARE SUBTRACTED FROM THE SUMMED AROMATIC RANGE, BUT NOT FROM THE UNADJUSTED C11-C22 AROMATIC RANGE.
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 9 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 0906(0.0-0.5) Sample ID :
08B22604
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Date
Analyst
RL
Analyzed
Lo
C9-C18 Aliphatics
mg/kg dry wt
ND
06/26/08
CJM
331
C19-C36 Aliphatics
mg/kg dry wt
998
06/26/08
CJM
331
Unadjusted C11-C22 Aromatics
mg/kg dry wt
391
06/26/08
CJM
331
C11-C22 Aromatics
mg/kg dry wt
391
06/26/08
CJM
331
Acenaphthene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Acenaphthylene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Anthracene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Benzo(a)anthracene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Benzo(a)pyrene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Benzo(b)fluoranthene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Benzo(g,h,i)perylene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Benzo(k)fluoranthene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Chrysene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Dibenzo(a,h)anthracene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Fluoranthene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Fluorene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Indeno(1,2,3-cd)pyrene
mg/kg dry wt
ND
06/26/08
CJM
1.2
2-Methylnaphthalene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Naphthalene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Phenanthrene
mg/kg dry wt
ND
06/26/08
CJM
1.2
Pyrene
mg/kg dry wt
ND
06/26/08
CJM
1.2
6/23/2008
06/26/08
CJM
Date Extracted EPH Solid
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
SPEC Limit Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 10 of 25
CONCORD, MA 01742
Purchase Order No.:
Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 0906(0.0-0.5) Analytical Method: MADEP-EPH-04-1 SAMPLES ARE EXTRACTED WITH METHYLENE CHLORIDE AND ACETONE BY PRESSURIZED FLUID EXTRACTION (SW846 3545) OR MICROWAVE (SW846 3546), EXCHANGED INTO HEXANE AND CONCENTRATED. ALIPHATIC AND AROMATIC FRACTIONS ARE SEPARATED. ANALYSIS IS BY GAS CHROMATOGRAPHY WITH FLAME IONIZATION DETECTION. PAH AND C11-C22 AROMATICS ARE DETERMINED IN THE METHYLENE CHLORIDE FRACTION. C9-C18 AND C19-C36 ALIPHATICS ARE DETERMINED IN THE HEXANE FRACTION. TARGET COMPOUND CONTRIBUTIONS ARE SUBTRACTED FROM THE SUMMED AROMATIC RANGE, BUT NOT FROM THE UNADJUSTED C11-C22 AROMATIC RANGE.
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 11 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 1016(0-0.5) Sample ID :
08B22599
Sample Matrix:
SOIL
‡Sampled : 6/18/2008 Not Specified
Units
Results
Date
Analyst
RL
Analyzed
Lo
C9-C18 Aliphatics
mg/kg dry wt
ND
06/25/08
CJM
36.8
C19-C36 Aliphatics
mg/kg dry wt
ND
06/25/08
CJM
36.8
Unadjusted C11-C22 Aromatics
mg/kg dry wt
65.8
06/25/08
CJM
36.8
C11-C22 Aromatics
mg/kg dry wt
56.0
06/25/08
CJM
36.8
Acenaphthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Acenaphthylene
mg/kg dry wt
0.3
06/25/08
CJM
0.2
Anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(a)anthracene
mg/kg dry wt
0.7
06/25/08
CJM
0.2
Benzo(a)pyrene
mg/kg dry wt
0.6
06/25/08
CJM
0.2
Benzo(b)fluoranthene
mg/kg dry wt
1.2
06/25/08
CJM
0.2
Benzo(g,h,i)perylene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
Benzo(k)fluoranthene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
Chrysene
mg/kg dry wt
1.0
06/25/08
CJM
0.2
Dibenzo(a,h)anthracene
mg/kg dry wt
0.2
06/25/08
CJM
0.2
Fluoranthene
mg/kg dry wt
1.2
06/25/08
CJM
0.2
Fluorene
mg/kg dry wt
0.2
06/25/08
CJM
0.2
Indeno(1,2,3-cd)pyrene
mg/kg dry wt
0.5
06/25/08
CJM
0.2
2-Methylnaphthalene
mg/kg dry wt
0.3
06/25/08
CJM
0.2
Naphthalene
mg/kg dry wt
0.3
06/25/08
CJM
0.2
Phenanthrene
mg/kg dry wt
0.7
06/25/08
CJM
0.2
Pyrene
mg/kg dry wt
1.3
06/25/08
CJM
0.2
6/23/2008
06/25/08
CJM
Date Extracted EPH Solid
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
SPEC Limit Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 12 of 25
CONCORD, MA 01742
Purchase Order No.:
Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 1016(0-0.5) Analytical Method: MADEP-EPH-04-1 SAMPLES ARE EXTRACTED WITH METHYLENE CHLORIDE AND ACETONE BY PRESSURIZED FLUID EXTRACTION (SW846 3545) OR MICROWAVE (SW846 3546), EXCHANGED INTO HEXANE AND CONCENTRATED. ALIPHATIC AND AROMATIC FRACTIONS ARE SEPARATED. ANALYSIS IS BY GAS CHROMATOGRAPHY WITH FLAME IONIZATION DETECTION. PAH AND C11-C22 AROMATICS ARE DETERMINED IN THE METHYLENE CHLORIDE FRACTION. C9-C18 AND C19-C36 ALIPHATICS ARE DETERMINED IN THE HEXANE FRACTION. TARGET COMPOUND CONTRIBUTIONS ARE SUBTRACTED FROM THE SUMMED AROMATIC RANGE, BUT NOT FROM THE UNADJUSTED C11-C22 AROMATIC RANGE.
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 13 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 1020(0.5-3.0) Sample ID :
08B22601
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Units
Results
Date
Analyst
RL
Analyzed
Lo
C9-C18 Aliphatics
mg/kg dry wt
ND
06/25/08
CJM
32.0
C19-C36 Aliphatics
mg/kg dry wt
ND
06/25/08
CJM
32.0
Unadjusted C11-C22 Aromatics
mg/kg dry wt
ND
06/25/08
CJM
32.0
C11-C22 Aromatics
mg/kg dry wt
ND
06/25/08
CJM
32.0
Acenaphthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Acenaphthylene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(a)anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(a)pyrene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(b)fluoranthene
mg/kg dry wt
0.2
06/25/08
CJM
0.2
Benzo(g,h,i)perylene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(k)fluoranthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Chrysene
mg/kg dry wt
0.3
06/25/08
CJM
0.2
Dibenzo(a,h)anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Fluoranthene
mg/kg dry wt
0.3
06/25/08
CJM
0.2
Fluorene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Indeno(1,2,3-cd)pyrene
mg/kg dry wt
ND
06/25/08
CJM
0.2
2-Methylnaphthalene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Naphthalene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Phenanthrene
mg/kg dry wt
0.3
06/25/08
CJM
0.2
Pyrene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
6/23/2008
06/25/08
CJM
Date Extracted EPH Solid
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
SPEC Limit Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 14 of 25
CONCORD, MA 01742
Purchase Order No.:
Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 1020(0.5-3.0) Analytical Method: MADEP-EPH-04-1 SAMPLES ARE EXTRACTED WITH METHYLENE CHLORIDE AND ACETONE BY PRESSURIZED FLUID EXTRACTION (SW846 3545) OR MICROWAVE (SW846 3546), EXCHANGED INTO HEXANE AND CONCENTRATED. ALIPHATIC AND AROMATIC FRACTIONS ARE SEPARATED. ANALYSIS IS BY GAS CHROMATOGRAPHY WITH FLAME IONIZATION DETECTION. PAH AND C11-C22 AROMATICS ARE DETERMINED IN THE METHYLENE CHLORIDE FRACTION. C9-C18 AND C19-C36 ALIPHATICS ARE DETERMINED IN THE HEXANE FRACTION. TARGET COMPOUND CONTRIBUTIONS ARE SUBTRACTED FROM THE SUMMED AROMATIC RANGE, BUT NOT FROM THE UNADJUSTED C11-C22 AROMATIC RANGE.
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 15 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 1078(3.0-6.0) Sample ID :
08B22602
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Units
Results
Date
Analyst
RL
Analyzed
Lo
C9-C18 Aliphatics
mg/kg dry wt
ND
06/25/08
CJM
30.8
C19-C36 Aliphatics
mg/kg dry wt
ND
06/25/08
CJM
30.8
Unadjusted C11-C22 Aromatics
mg/kg dry wt
ND
06/25/08
CJM
30.8
C11-C22 Aromatics
mg/kg dry wt
ND
06/25/08
CJM
30.8
Acenaphthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Acenaphthylene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(a)anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(a)pyrene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(b)fluoranthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(g,h,i)perylene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(k)fluoranthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Chrysene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Dibenzo(a,h)anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Fluoranthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Fluorene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Indeno(1,2,3-cd)pyrene
mg/kg dry wt
ND
06/25/08
CJM
0.2
2-Methylnaphthalene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Naphthalene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Phenanthrene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Pyrene
mg/kg dry wt
ND
06/25/08
CJM
0.2
6/23/2008
06/25/08
CJM
Date Extracted EPH Solid
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
SPEC Limit Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 16 of 25
CONCORD, MA 01742
Purchase Order No.:
Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 1078(3.0-6.0) Analytical Method: MADEP-EPH-04-1 SAMPLES ARE EXTRACTED WITH METHYLENE CHLORIDE AND ACETONE BY PRESSURIZED FLUID EXTRACTION (SW846 3545) OR MICROWAVE (SW846 3546), EXCHANGED INTO HEXANE AND CONCENTRATED. ALIPHATIC AND AROMATIC FRACTIONS ARE SEPARATED. ANALYSIS IS BY GAS CHROMATOGRAPHY WITH FLAME IONIZATION DETECTION. PAH AND C11-C22 AROMATICS ARE DETERMINED IN THE METHYLENE CHLORIDE FRACTION. C9-C18 AND C19-C36 ALIPHATICS ARE DETERMINED IN THE HEXANE FRACTION. TARGET COMPOUND CONTRIBUTIONS ARE SUBTRACTED FROM THE SUMMED AROMATIC RANGE, BUT NOT FROM THE UNADJUSTED C11-C22 AROMATIC RANGE.
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 17 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 1130(0-0.5) Sample ID :
08B22600
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Units
Results
Date
Analyst
RL
Analyzed
Lo
C9-C18 Aliphatics
mg/kg dry wt
ND
06/25/08
CJM
30.9
C19-C36 Aliphatics
mg/kg dry wt
ND
06/25/08
CJM
30.9
Unadjusted C11-C22 Aromatics
mg/kg dry wt
ND
06/25/08
CJM
30.9
C11-C22 Aromatics
mg/kg dry wt
ND
06/25/08
CJM
30.9
Acenaphthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Acenaphthylene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(a)anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(a)pyrene
mg/kg dry wt
0.2
06/25/08
CJM
0.2
Benzo(b)fluoranthene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
Benzo(g,h,i)perylene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Benzo(k)fluoranthene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Chrysene
mg/kg dry wt
0.3
06/25/08
CJM
0.2
Dibenzo(a,h)anthracene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Fluoranthene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
Fluorene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Indeno(1,2,3-cd)pyrene
mg/kg dry wt
ND
06/25/08
CJM
0.2
2-Methylnaphthalene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Naphthalene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Phenanthrene
mg/kg dry wt
ND
06/25/08
CJM
0.2
Pyrene
mg/kg dry wt
0.4
06/25/08
CJM
0.2
6/23/2008
06/25/08
CJM
Date Extracted EPH Solid
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
SPEC Limit Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 18 of 25
CONCORD, MA 01742
Purchase Order No.:
Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 1130(0-0.5) Analytical Method: MADEP-EPH-04-1 SAMPLES ARE EXTRACTED WITH METHYLENE CHLORIDE AND ACETONE BY PRESSURIZED FLUID EXTRACTION (SW846 3545) OR MICROWAVE (SW846 3546), EXCHANGED INTO HEXANE AND CONCENTRATED. ALIPHATIC AND AROMATIC FRACTIONS ARE SEPARATED. ANALYSIS IS BY GAS CHROMATOGRAPHY WITH FLAME IONIZATION DETECTION. PAH AND C11-C22 AROMATICS ARE DETERMINED IN THE METHYLENE CHLORIDE FRACTION. C9-C18 AND C19-C36 ALIPHATICS ARE DETERMINED IN THE HEXANE FRACTION. TARGET COMPOUND CONTRIBUTIONS ARE SUBTRACTED FROM THE SUMMED AROMATIC RANGE, BUT NOT FROM THE UNADJUSTED C11-C22 AROMATIC RANGE.
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 19 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 0637(3.0-6.0) Sample ID :
08B22605
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Results
Units
Date
Analyst
RL
Analyzed Lead
mg/kg dry wt
226
SPEC Limit Lo
06/25/08
OP
0.92
Date
Analyst
RL
P/ F
Hi
Field Sample # : 0692(0.5-2.0) Sample ID :
08B22603
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Analyzed Lead
mg/kg dry wt
49100
SPEC Limit Lo
06/25/08
OP
0.93
Date
Analyst
RL
P/ F
Hi
Field Sample # : 0694(0.5-3.0) Sample ID :
08B22606
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Analyzed Lead
mg/kg dry wt
27500
SPEC Limit Lo
06/25/08
OP
0.98
Date
Analyst
RL
P/ F
Hi
Field Sample # : 0906(0.0-0.5) Sample ID :
08B22604
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Analyzed Lead
mg/kg dry wt
9520
SPEC Limit Lo
06/25/08
OP
0.83
P/ F
Hi
Field Sample # : 1016(0-0.5) Sample ID :
08B22599
Sample Matrix:
SOIL
‡Sampled : 6/18/2008 Not Specified
Lead
Units
Results
Date Analyzed
Analyst
RL
mg/kg dry wt
107
06/25/08
OP
0.92
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
SPEC Limit Lo Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 20 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 1020(0.5-3.0) Sample ID :
08B22601
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Results
Units
Date
Analyst
RL
Analyzed Lead
mg/kg dry wt
1670
SPEC Limit Lo
06/25/08
OP
0.80
Date
Analyst
RL
P/ F
Hi
Field Sample # : 1078(3.0-6.0) Sample ID :
08B22602
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Units
Results
Analyzed Lead
mg/kg dry wt
21.7
SPEC Limit Lo
06/25/08
OP
0.77
Date
Analyst
RL
P/ F
Hi
Field Sample # : 1130(0-0.5) Sample ID :
08B22600
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Units
Results
Analyzed Lead
mg/kg dry wt
553
06/25/08
SPEC Limit Lo
OP
0.78
Analytical Method: SW846 3050/6010 SAMPLES ARE DIGESTED WITH NITRIC ACID AND THEN ANALYZED BY INDUCTIVELY COUPLED PLASMA EMISSION SPECTROSCOPY.
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 21 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 0637(3.0-6.0) Sample ID :
08B22605
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Results
Units
Date
Analyst
RL
Analyzed Solids, total
%
81.9
SPEC Limit Lo
06/24/08
JJB
Date
Analyst
P/ F
Hi
Field Sample # : 0692(0.5-2.0) Sample ID :
08B22603
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
RL
Analyzed Solids, total
%
81.0
SPEC Limit Lo
06/24/08
JJB
Date
Analyst
P/ F
Hi
Field Sample # : 0694(0.5-3.0) Sample ID :
08B22606
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
RL
Analyzed Solids, total
%
76.7
SPEC Limit Lo
06/24/08
JJB
Date
Analyst
P/ F
Hi
Field Sample # : 0906(0.0-0.5) Sample ID :
08B22604
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
RL
Analyzed Solids, total
%
90.8
SPEC Limit Lo
06/24/08
JJB
P/ F
Hi
Field Sample # : 1016(0-0.5) Sample ID :
08B22599
Sample Matrix:
SOIL
‡Sampled : 6/18/2008 Not Specified
Solids, total
Units
Results
Date Analyzed
Analyst
%
81.6
06/24/08
JJB
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC Limit Lo Hi
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
RL
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 22 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 1020(0.5-3.0) Sample ID :
08B22601
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Results
Units
Date
Analyst
RL
Analyzed Solids, total
%
94.0
SPEC Limit Lo
06/24/08
JJB
Date
Analyst
P/ F
Hi
Field Sample # : 1078(3.0-6.0) Sample ID :
08B22602
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Units
Results
RL
Analyzed Solids, total
%
97.6
SPEC Limit Lo
06/24/08
JJB
Date
Analyst
P/ F
Hi
Field Sample # : 1130(0-0.5) Sample ID :
08B22600
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Units
Results
Analyzed Solids, total
%
97.4
06/24/08
RL
SPEC Limit Lo
JJB
Analytical Method: SM 2540G PERCENT OF SAMPLE REMAINING AFTER DRYING OVERNIGHT AT 103-105 DEGREES CENTIGRADE.
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
Hi
P/ F
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 23 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 0637(3.0-6.0) Sample ID :
08B22613
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Results
Units
Date
Analyst
RL
Analyzed Lead
mg/l leachate
0.170
SPEC Limit Lo
06/26/08
OP
0.015
Date
Analyst
RL
P/ F
Hi 5
P
Field Sample # : 0692(0.5-2.0) Sample ID :
08B22611
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Analyzed Lead
mg/l leachate
145
SPEC Limit Lo
06/26/08
OP
0.015
Date
Analyst
RL
P/ F
Hi 5
F
Field Sample # : 0694(0.5-3.0) Sample ID :
08B22614
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Analyzed Lead
mg/l leachate
12.9
SPEC Limit Lo
06/26/08
OP
0.015
Date
Analyst
RL
P/ F
Hi 5
F
Field Sample # : 0906(0.0-0.5) Sample ID :
08B22612
Sample Matrix:
SOIL
‡Sampled : 6/20/2008 Not Specified
Units
Results
Analyzed Lead
mg/l leachate
55.6
SPEC Limit Lo
06/26/08
OP
0.015
P/ F
Hi 5
F
Field Sample # : 1016(0-0.5) Sample ID :
08B22607
Sample Matrix:
SOIL
‡Sampled : 6/18/2008 Not Specified
Lead
Units
Results
Date Analyzed
Analyst
RL
mg/l leachate
0.022
06/26/08
OP
0.015
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
SPEC Limit Lo Hi 5
P/ F P
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 24 of 25 Purchase Order No.:
CONCORD, MA 01742 Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
Field Sample # : 1020(0.5-3.0) Sample ID :
08B22609
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Results
Units
Date
Analyst
RL
Analyzed Lead
mg/l leachate
3.74
SPEC Limit Lo
06/26/08
OP
0.015
Date
Analyst
RL
P/ F
Hi 5
P
Field Sample # : 1078(3.0-6.0) Sample ID :
08B22610
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Units
Results
Analyzed Lead
mg/l leachate
0.128
SPEC Limit Lo
06/26/08
OP
0.015
Date
Analyst
RL
P/ F
Hi 5
P
Field Sample # : 1130(0-0.5) Sample ID :
08B22608
Sample Matrix:
SOIL
‡Sampled : 6/19/2008 Not Specified
Units
Results
Analyzed Lead
mg/l leachate
1.77
06/26/08
SPEC Limit Lo
OP
0.015
Analytical Method: SW846 1311/6010 SAMPLES ARE EXTRACTED INTO pH 5.0 BUFFER FOR 18-24 HOURS AND THEN ANALYZED BY INDUCTIVELY COUPLED PLASMA EMISSION SPECTROMETRY. WATER SAMPLES ARE FILTERED, NOT EXTRACTED.
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
P/ F
Hi 5
P
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 ELISSA BROWN EARTH TECH - CONCORD
6/27/2008
300 BAKER AVE., SUITE 290
Page 25 of 25
CONCORD, MA 01742
Purchase Order No.:
Project Location:
MBTA-READVILLE
LIMS-BAT #:
LIMT-17022
Date Received:
6/20/2008
Job Number:
63728
** END OF REPORT **
RL = Reporting Limit ND = Not Detected at or above the Reporting Limit
SPEC LIMIT = a client specified recommended or regulatory level for comparison with data to determine PASS (P) or FAIL (F) condition of results.
NM = Not Measured * = See end of report for comments and notes applying to this sample ‡ = See attached chain-of-custody record for time sampled
39 Spruce Street ° East Longmeadow, MA 01028 ° FAX 413/525-6405 ° TEL. 413/525-2332 QC SUMMARY REPORT SAMPLE QC: Sample Results with Duplicates Sample Matrix Spikes and Matrix Spike Duplicates
BATCH QC: Lab fortified Blanks and Duplicates Standard Reference Materials and Duplicates Method Blanks
Report Date: QC Batch Number: Sample Id
6/27/2008
Lims Bat # :
LIMT-17022
Page 1 of 16
GC/FID-21506
Analysis
QC Analysis
Values
Units
Limits
08B22599 2-Fluorobiphenyl
Surrogate Recovery
112.2
%
40-140
2-Bromonaphthalene
Surrogate Recovery
114.2
%
40-140
Chlorooctadecane
Sur. Recovery
70.6
%
40-140
Terphenyl
Sur. Recovery
84.9
%
40-140
2-Fluorobiphenyl
Surrogate Recovery
115.1
%
40-140
2-Bromonaphthalene Chlorooctadecane
Surrogate Recovery Sur. Recovery
115.4 63.4
% %
40-140 40-140
Terphenyl
Sur. Recovery
79.3
%
40-140
Naphthalene
Blank